GCMS unknown compound analysis, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031702\5302.D Vial: 16 Acq On : 17 Mar 2002 9:02 pm Operator: McLean Sample : 3/11/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 1.17 ug/L 437107 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 76 3 Benzoic acid, 2,5-bis(trimethyls... 370 C16H30O4Si3 003618-20-0 47 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 40 Abundance Scan 989 (12.046 min): 5302.D (-) m/z 73.10 100.00%' 7(3 I 5000 267 355 45 11.80 12.00 12.20 12.40 108 133154 193 223 323 . I m/z 267.00 35.97% 0^ ' I ' m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cyclopentasiloxane, decamethyl- 7(3

355 267 5000 n 11.80 12.00 12.20 12.40 m/z 355.10 24.08%

45 207 323 I 0 fn/z-> 50 100 150 200 250 300 350 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

11.80 12.00 12.20 12.40 5000 m/z 268.00 8.90% 267

355 45 96 133 165 1^3 223 247 293 323 0 m/z-> 50 100 150 200 250 300 350 Abundance #313246: Benzoic acid, 2,5-bis(trimethylsiloxy)-. trimethy... 7(3 11.80 12.00 12.20 12.40 355 m/z 356.00 8.57%'

5000

45

0 15 J 105 MH 147 179 223 267 297 m/z-> 50 100 150 200 250 300 350 11.80 12.00 12.20 12.40

5302.D 5080302.M Mon Mar 25 06:56:29 2002 Page 4

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