GCMS analysis results for sample AE03798, March 29, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report t Data File : C:\MSDCHEM\l\DATA\031202\3798.D Vial: 63 Acq On : 13 Mar 2002 8:46 am Operator: McLean Sample : SAMPLE 3798 2/19/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 12.06 0.58 ug/L 289294 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 46 3 Benzeneacetic acid, .alpha.,4-bi... 384 C17H3204Si3 037148-64-4 38 4 Benzoic a. d, 2-[(trimethylsilyl. .. 282 C13H2203Si2 003789-85-3 38 Abundance Scan 990 (12.055 mln): 3798.D (-) m/z 73.10 100.00% 73

5000 267 355 ■ ■ i • • ■ ■ i -PPP 11.80 12.00 12.20 12.40 0- 45 ■ - IIIt 133154 1?3 223 , 323 1 m/z 267.00 47.30% m/z-> 50 100 150 200 250 300 350 400 Abundance #3130 y .. .■ ...., decamethyl- 73

355 267 5000 “ 11.80 12.00 12.20 12.40 ' m/z 355.10 34.42% 45 207 323 4 ti — 0- • • i • • • . । * ■ > r' miz-> 50 100 150 200 250 300 350 400 Abundance #313065: Cyck decamethyl- 73

mIPTT 11.80 12.00 12.20 12.40 m/z 356.10 12.96% 5000 267 355 45 0- • • 1 , 96 , ,133 165.123 223244 . 293 323 . m/z-> 50 100 ' 150 200 250 300 350 1400 Abundance #322334: Benzeneacetic acid, .alpha., 4-bis[(trimethylsilyl... 73 T Ti T T 267 11.80 12.00 12.20 12.40 m/z 268.00 9.26%

5000

45 147 , 10512%, . 168 123214237, 12983171 369390 m/z—> 0 ' so”’ 100 150 200 250 TTr TIT 300 350 400 i1 • • ‘ i T 11.80 12.00 12.20 12.40 T

3798.D 5080302.M Fri Mar 15 14:27:34 2002 Page 3

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