GCMS unknown compound analysis, sample AE05514, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031702\5514.D Vial: 15 ' Acq On : 17 Mar 2002 8:13 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 1.58 ug/L 557821 Naphthalene-d8 13.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 58 3 N-(Trifluoroacetyl)-0,0',0''-tri... 481 C19H34F3NO4Si3 000000-00-0 47 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 000000-00-0 38 Abundance Scan 989 (12.047 min): 5514,D (-) m/ z 73.10 100.00% 7|3 I 5000 267 355 ■'“'H

45 11.80 12.00 12.20 12.40 125 ' i ■' I ' ' 154 ‘''' .■'?3 223 j ^i"' '' ’ ' f ' 323^ m/z 267.00 34.15% 0 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 K -fn-P 11.80 12.00 12.20 12.40 355 m/z 355.10 24.36% 45 103 133 165^3 223^ | | 293 323 [....................... 0 J I ■n/z-> 50 100__ 150 200 250 300 350 400 450 Abundance #313068; Cyclopentasiloxane, decamethyl- 7i3

355 11.80 12.00 12.20 12.40 267 m/z 74.10 8.91% 5000

45 207 323, 0 Tl/Z~> 50 100 150 200 250 300 350 400 450 Abundance #364172; N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)... 73 11.80 12.00 12.20 12.40 m/z 268.00 8.78% 355

5000

45 J ), 120147 193 236265 [ 481 0 ~r-t-r m/z-> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

5514.D 5080302.M Mon Mar 25 06:55:09 2002 Page 4

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