GCMS unknown compound analysis, sample AE05305, March 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\031702\5305.D Vial: 8 Acq On 17 Mar 2002 2:31 pm Operator: McLean Sample 3/11/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N. L ********************************************************************* Peale Number 2 Cyciopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.06 0.69 ug/L 280018 Naphthalene-de 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 43 3 N-(Trifluoroacetyl)-N,O,O',0''-t... 553 C22H42F3NO4Si4 000000-00-0 38 £J42LiZ£iIlH2£^££tyn-2 i O\OJ2-tris;^^^ 495 C20H3^3NO4Si3 054135-51-2 38 Abundance Scan 990 (12.056 min); 5305.D (-) m/z 73.10 100.00% 73

5000 267 355

T 11.80 12.00 12.20 12.40 154 193223 , 323 m/z 267.00 44.70%! 0 T-e-n-y nfi/z-> 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyciopentasiloxane, decamethyi- 73

355 267 5000 11.80 12.00 12.20 12.40 m/z 355.10 38.23%

207 0 ■’-T’ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #331718: Phenethylamine, N-methvl-.beta.,3,4-lris(lrim6thy.., 73

.................. .......................... 11.80 12.00 12.20 12.40 5000 m/z 356.00 11.77% 355 .1 11 'I. y ,^37^57 ,309 384 0^ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #377151: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethyl... 713 11.80 12.00 12.20 12.40 m/z 268.00 11.37% 355 5000

n/z-> 0 41# 50 , 116^1 "*7 193 236267 100 150 200 250 300 350 400 450 500 550 | L 11.80 12.00 12.20 12.40

5305.D 5080302.M Mon Mar 25 06:48:22 2002 Page 4

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