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GCMS analysis results for sample AE02381, March 2002

Machine-extracted title · confidence 100%

Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.

NYC-WTC_000010659–000010676

Folder label: “GCMS X 1/31/02 A 3/4/02

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Scanned page image, NYC-WTC_000010666
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2381.D Vial: 16 Acq On 4 Mar 2002 10:32 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

12.07 1.12 ug/L 464954 Naphthalene-d8 13.05

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H30O3Si5 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H30OJ Si5, 000541-02-6 76 3 Benzeneethanamine, N-[ (pentaf luo... 563 C24H34FNO3Si3 055429-13-5 43 4 N-(Trifluoroacetyl)-N,0,0',0**-t... 553 C22H42F3N94Si4 000000-00-0 38 Abundance Scan 992 (12.074 min): 2381 .D (-) m/z73.10 100.00% 73

5000 267 355 '11 ''1' I TTTTT 11.80 12.00 12.20 12.40 0- - • ■ i1 ***I 108 154 193223 Mhdutfaenjuntjia *+ j -zz3 , 323 m/z 267.00 35.18% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 IIPTT ■ I ■ ■ ■ ' I ■' 11.80 12.00 12.2012.40 m/z 355.10 24.12%

207 323 0- ' ■ i ■1 • ■ i ■ inyudik; 1'1 I T T T mtz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 ■ ■ i ■'' • i ' 1........ TT 11.80 12.00 12.20 12.40 5000 m/z 356.10 8.86% 267 355

0-241 103133163193223 । | 323 i | i r. l । । । ( . n/z-> 50 ______________________ 100 150 200 250 300 ____________________ 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentafluorophenyl)methylen... Tpp ■ ■ i ■ ■ ■ • i ■ ■ 73 355 11.80 12.00 12.20 12.40 m/z 268.00 8.06%

5000

117147177207 251281 0 . 444 4 i THfmmpe - 386 458 548 I I I J* I » I » » » ’ > j1 I* »

/z—> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

2381.D 5080302.M Mon Mar 18 08:33:19 2002 Page 3

NYC-WTC_000010666

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NYC-WTC_000010666Source: NYC Law Department, mirrored locally

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