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GCMS analysis report, sample AE04380, April 2, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry results for sample AE04380 analyzed on April 2, 2002.

NYC-WTC_000012461–000012469

Folder label: “GCMS X 3-1-02 A 3-27-02

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NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\1\DATA\032602\4380FB.D Vial: 33 Acq On : 27 Mar 2002 7:41 am Operator: McLean Sample : SAMPLE 4380 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.05 0.58 ug/L 289415 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 91 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 62 3 Benzeneethi Famine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 38 4 Benzeneeth namine, N-[(pentafluo... 475 C21H26F5NO2Si2 055429-85-1 38 Abundance 7 Scan 1527 (12.051 mln): 4380FB.D (-) m/z73.10100.00%

5000 267 355 —PPP 11.80 12.00 12.20 12.40 *yzz3 3 * 193223 154 323 * ■ ■ ■ i ■ ■ ■ ■ i • • • ■ i ■ • ■ ■ i ■1 m/z 267.00 35.08% 0-44 __tad_ _ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ‘ ■ I ‘11 1 i ■ PPpm*pp— 11.80 12.00 12.20 12.40 m/z 355.10 26.46%

207 , 323 323 0- 1’1109*011**pmmmmm]r ■I I"’’ '111 " I ‘' n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

i ‘ ■11 W ■ • • i T 11.80 12.00 12.20 12.40 5000 m/z 356.00 10.54% 267 355

281 < 103133163193223 1 323 0-- —Tm9n—’t0o.unenma —939BenTu1 TTnnUutar /z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #378300: Benzeneethanamine, N-[(pentefluorophenyl)methylen... 73 355 11.80 12.00 12.20 12.40 m/z 268.00 10.53%

5000

0-44+ , 117147177207 251281 -386TI9PPTTTTT 458 548 i ■'' ■ i 4 T n/z—> 50 100 150 200 250 300 350 400 450 500 550 11.80 12.00 12.20 12.40

4380FB.D 5080302.M Wed Mar 27 09:27:52 2002 Page 3

NYC-WTC_000012468

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NYC-WTC_000012468Source: NYC Law Department, mirrored locally

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