GCMS unknown compound analysis, sample AE05308, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\O317O2\53O8FB.D Vial: 11 Acq On : 17 Mar 2002 4:58 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 5.57 1.39 ug/L 411900 1,4-Dichlorobenzene-d4 9.55 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 36 2 1-Propene-l-thiol 74 C3H6S 000925-89-3 9 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 9 4 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 _____ 015745-87-6 9 Abundance Scan 275 (5.570 min); 5308FB.D (-) m/z 73.10 100.00% 7)3

5000

45 5.20 5.40 5.60 5.80 6.00 i| 8,7 103 m/z 45.10 14.13% Ol ) " " 1" " I'' * ‘ I I “ " I" " I m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #9702: Butane, 2-methoxy-2-methyl- S$ Ether, methyl tert-p... 73

5000 5.20 5.40 5.60 5.80 6.00 43 55 m/z 71.10 7.13% 87

m/z->. 0 29

20 30 40 50 60 70 80 90 100110120130140150160170180 ft flibundance #2002: 1-Propene-1-thiol 7i3

4 5.20 5.40 5.60 5.80 6.00 5000 m/z 87.10 4.34%

43

Ol 'n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyrester 7)3 5.20 5.40 5.60 5.80 6.00 m/z 69.10 4.33%

5000

43 27 55 87 113 131 174 0 J. P ltTrpn\ m/z-> 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 5.20 5.40 5.60 5.80 6.00

i308FB.D 5080302.M Mon Mar 25 06:51:27 2002 Page 3

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