GCMS unknown compound analysis, sample AE05306, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\l\DATA\031702\5306.D Vial: 9 Acg On : 17 Mar 2002 3:20 pm Operator: McLean Sample : 3/11/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 1.43 ug/L 460050 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 36 2 3-Pentanol, 2,4-dimethyl- $$ Dii... 116 C7H16O 000600-36-2 9 . 3 Acetic acid, 3-[1,3]dioxolan-2-y. . . 174 C8H14O4 000000-00-0 9 4 3-Pentanol, 2L±:djjnethyl-_(CAS)^^^_216_C7H160 000600-36-2 9 Abundance Scan 274 (5.561 min): 5306.D (-) m/z 73.10 100.00% 7|3

5000

I '-TTi-ri 45 5.20 5.40 5.60 5.80 0 I ' 1 ' ' ' ' I ' ' ' ' I ' ' ' ,1. 87 103 m/z 45.10 13.42% m/z-> 20 40 60 80 100 120 140 160 180 Abundance #9702: Butane, 2-methoxy-2-methyl- S$ Ether, methyl tert-p... 73

5000 ............. k I' 5.20 5.40 5.60 5.80 '*3 55 87 m/z 71.10 8.16% 29

'n/z-> 0^ Ukt 20 40 '"i ' ' I ' I ' 60 80 100 120 140 160 180 Abundance #17064: 3-Penlanol. 2,4-dimethyl- S$ Diisopropylcarbinol S... 73

5.20 5.40 5.60 5.80 5000 43 m/z 74.10 5.05%

27

k 15 85 97 114 0 Ti/z-> 20 40 60 80 100 120 140 160 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 713 5.20 5.40 5.60 5.80 m/z 87.10 4.43%

43 27 55 87 113 131 174 0 ' I ' 'I''" k I ' ' ' I ' m/z-> 20 40 60 80 100 120 140 160 180 5.20 5.40 5.60 5.80

5306.D 5080302.M Mon Mar 25 06:49:20 2002 Page 3

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