GCMS unknown compound analysis, sample AE05306, March 2002

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Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\031702\5306.D Vial: 9 Acq On : 17 Mar 2002 3:20 pm Operator: McLean Sample : 3/11/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Cydopentasiloxane, decamet... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

12.05 1.42 ug/L 620227 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 52 3 3,4-Dihydroxybenzyl alcohol,tris... 356 C16H32O3Si3 068595-79-9 47 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 47 <\bundance Scan 989 (12.046 min): 5306.D (-) ririTz 73.10 100.00% 73

5000 267 355 45 11.80 12.00 12.20 12.40 103125 154 193 223 323 m/z 267.00 35-20% 0 ' I'"' ' ’ ' ' i’ m/z-> 50 100 150 200 250 300 350 Abundance #313068: Cydopentasiloxane, decamethyl- 7(3

355 267 5000 11.80 12,00 12.20 12.40 m/z 355.10 24.93%

207 0 —iN—»— m/z-> 100 150 200 250 300 350 Abundance #313.065: Cyclopentasiloxane, decamethyl- 73

11.80 12.00 12.20 12.40 5000 m/z 356.10 9.60% 267

355 45 Uu 96 133 165 193 223 247 293 323 0 '' 'i' •v-r-j-T—r-i—T-f-T—t ■n/z-> 50 100 150 200 250 300 350 Abundance #302823: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 7(3 11.80 12.00 12.20 12.40 m/z 74.10 9.21%

267 2E3 179 356 45 147

■n/z-> 0 50 103 I ' 100 A150 209 237 . 200 250 312 300 350 s 11.80 12.00 12.20 12.40

;306.D 5080302.M Mon Mar 25 06:49:21 2002 Page 4

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