NYC-WTC_000011285
Laboratory report showing GCMS analysis of environmental sample AE03258 on April 3, 2002 with surrogate recovery data.
Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis results for sample AE03253, April 2002
Machine-extracted title · confidence 100%Laboratory report showing GCMS analysis of environmental sample AE03253 conducted on April 3, 2002.
NYC-WTC_000011219–000011240Folder label: “GCMS X 2/13/02 A 3/2/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
,* Data File C:\MSDCHEM\l\DATA\022802\03253.D Vial: 20 Acq On 2 Mar 2002 4:42 am Operator: McLean Sample 2/13/02 GC SCAN Inst : Instrumen 'Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080202.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.59 2.71 ug/L 855233 1,4-Dichlorobenzene-d4 9.58
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 28 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 9 3 3- (CYCLOHEX-3 1 -EN-YL) PROPANOL $$ . . . 174 C8H14O4 015745-87-6 9 4 1-Propene-l-thiol 74 C3H6S 000925-89-3 9 Abundance Scan 277 (5.588 min): 03253.D (-) m/z 73.10 100.00%| 73
5000
I I I ll I I *4* < T 111 ■ 45 5.20 5.40 5.60 5.80 6.00 1 5587 103 i m/z 45.10 14.80% 01 . rt ,p'..,1।।i(...,j(।।. m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73
5000 5.20 5.40 5.60 5.80 6.00 43 55 87 m/z 71.10 7.84% 29 Of * p > A . . . । nw 111 r 11.1111111111 p i > ■ p 1111111111111 j । i'ti । 'r. 11'11 r. 11 it r i p i m/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #78238: Acetic acid, 3-(1,3]dioxolan-2-ylpropyl ester 73 ‘I T T Its 5.20 5.40 5.60 5.80 6.00 5000 m/z55.10 5.14%
43 27 55 87 113 131 174 mmtmnpe 0 bp. T ■. Plt 11 ■ I'l'i 11 > | "T‘ > > 11 > i’r 1111111111 rri 11111111 n || 111. | ■ I > 11111111 n par iz-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 +14+**1****s-**‘t** 5.20 5.40 5.60 5.80 6.00 m/z 69.10 4.83%
5000
43
01 ..■ 27, ..a 55 .....J, 87...... 113... 131............174 TT i • ■ ■ ■ i /z—> 20 30 40 50 60 70 80 90 100110120130140150160170180 5.20 5.40 5.60 5.80 6.00
03253.D 5080202.M Tue Apr 02 12:02:07 2002 Page 3
NYC-WTC_000011226
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NYC-WTC_000011226Source: NYC Law Department, mirrored locally
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