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GCMS analysis report for sample AE02334, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010488–000010512

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\03 0402\2152 . D Vial: 6 Acq On 4 Mar 2002 2:21 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L Peak Number 6 Benzoic acid, 4-ethoxy-, et... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T. 18.79 0.54 ug/L 292625 Acenaphthene-dl0 18.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 4-ethoxy-, ethyl e... 194 C11H1403 023676-09-7 96/ 2 Benzoic acid, 4-ethoxy-, ethyl e... 194 C11H1403 023676-09-7 94 3 Ethylparaben $$ Benzoic acid, 4-... 166 C9H10O3 000120-47-8 60 4 Benzoic acid, 4-hydroxy-, ethyl ... 166 C9H10O3 000120-47-8 60 Abundance Scan 1733 (18.795 min): 2152.D (-) m/z 121.10 100.00% 121

5000 149

65 138 194 93 166 18.40 18.60 18.80 19.00 19.20 50 , 76 m/z 149.10 47.52% 0+ -4, i, - 4/1r4hi 4*4 109 ’ t > .4 > I ’* • • | • • . • | * m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #105824: Benzoic acid, 4-ethoxy-, ethyl ester 121

149 5000 194 18.40 18.60 18.80 19.00 19.20 65 138 m/z 194.10 28.66% 93 166 50 . 76 1 109 L 179 Ol miz-> 20 40 60 80 100 120 140 160 180 200 Abundance #105823: Benzoic acid, 4-ethoxy-, ethyl ester $$ Benzoic a... 121

j • • • » I • > a 149 18.40 18.60 18.80 19.00 19.20 5000 m/z 65.10 27.67% 138 194 29 65 93 166 01 15 1 1.50 J 76 1 109 PPPTT 1 . t l 179 _ I (, • ■ i1 1 ■ i • ■ ' * i m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #67028: Ethylparaben $$ Benzoic acid, 4-hydroxy-, ethyl es... 121 18.40 18.60 18.80 19.00 19.20 m/z 138.00 27.18%

5000

138 166 39 65 93 m/z-> 0 —2758,+81119L 140| 151160[ 180 200 20 40 60 80 100 120 18.40 18.60 18.80 19.00 19.20

2152.D 5080302.M Mon Mar 18 08:30:28 2002 Page 8

NYC-WTC_000010500

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NYC-WTC_000010500Source: NYC Law Department, mirrored locally

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