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GCMS analysis report for sample AE02334, March 2002

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Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010488–000010512

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report . Data File C:\MSDCHEM\1\DATA\ 03 04 02\2152.D Vial: 6 Acq On 4 Mar 2002 2:21 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C: \DATABASE\WILEY7N. L ********************************************************************* Peak Number 7 Benzoic acid, 2,4-bis[(trim... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 20.31 3.22 ug/L 1737520 Acenaphthene-dl0 18.17 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4S13 010586-16-0 38 2 n-Nonadecanoic acid, pentamethyl... 428 C24H5202Si2 000000-00-0 35 3 Silanol, trimethyl-, triester wi... 278 C9H27BO3Si3 004325-85-3 27 4 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 25 Abundance Scan 1900 (20.309 min): 2152.D (-) m/z 73.10 100.00% 73

5000 147 355 221 281 T T T T I 401 20.00 20.20 20.40 20.60 45 117 191 191, 249, 327 30.57% — m/z 355.10 0- 1 15 *i *+i —14 Pinr .A 1 m/z-> 50 100 150 200 250 300 350 400 Abundance #313243: Benzoic acid. 2,4-bis[(trimethylsilyl)oxy]-, trim... 73

5000 355 • ■ i ■ ■ • • i ■ IIIWPPIUTT 20.00 20.20 20.40 20.60 45 m/z 147.10 26.67%

16. t „ 0- . , t “i't r 1051334183,1934233,251241. 2214 . miz-> 50 100 150 200 250 300 350 400 Abundance #346318: n-Nonadecanoic acid, pentamethyldisilyl ester 43 73 355

T T ’I T 1 20.00 20.20 20.40 20.60 147 m/z 221.10 22.99% 5000 413 203

m/z-> 0- LulL . I b. ,245.295,325 .... K 50 100 150 ir 200 250 300 350 400 Abundance #222510: Silanol, trimethyl-, triester with boric acid (H3... 73 ’ T —1 T 20.00 20.20 20.40 20.60 I 221 m/z 281.00 15.25%

5000

263 45

m/z—> 0 ■ ■ 50 i ) —344. 133

100 150 175

200 1 1 1 '' 1 1 i ' 1 1 ' i ■ ■ ■ ■ l ■ 250 300 350 400 ■ ■ i • ■ ■ ■ i' oonapanss/ 20.00 20.20 20.40 20.60

2152.D 5080302.M Mon Mar 18 08:30:30 2002 Page 9

NYC-WTC_000010501

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NYC-WTC_000010501Source: NYC Law Department, mirrored locally

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