NYC 9/11 Public Portal Document
Library Search Compound Report
. Data File : C:\MSDCHEM\1\DATA\030402\2152.D Vial: 6
Acq On : 4 Mar 2002 2:21 pm Operator: McLean
Sample : 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 8 Iron, monocarbonyl-(1,3-but... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.41 2.64 ug/L 1404560 Phenanthrene-dl0 22.53
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 83
2 BISTRIMETHYLSILYL N-ACETYL EICOS. . . 511 C28H57NO3Si2 000000-00-0 45
3 1,1,1,5,7,7, 7-Heptamethyl-3,3-bi... 444 C13H40O5S16 038147-00-1 42
4 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 42
Abundance Scan 2132 (22.414 min): 2152.D (-) m/z 73.10 100.00%
73
5000
147
221
281 355 429 22.00 22.20 22.40 22.60 22.80
- m/z 147.10 30.42%
0-— p*r mmmmpmmmmmmmg
m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650
Abundance #350342: Iron, monocarbonyl-(1,3-butediene-1.4-dlcarix>nic ...
73
147 221
5000 355 22.00 22.20 22.40 22.60 22.80
281 429 m/z 221.10 22.03%
26 111 503
/z—>
0 .h/u834/, — 43174/4.7 ftmme
577 652
50 100 150 200 250 300 350 400 450 500 550 600 650
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dlf l
73
T‘ i ■»> * i > > • > i»■ • ■ i
22.00 22.20 22.40 22.60 22.80
5000
m/z 429.10 11.11%
174
129 337
221 281 , 429
0- 44 **13901., i' • ■ ■ i ■ " • i ■" ■ i
m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650
Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy...
73 22.00 22.20 22.40 22.60 22.80
m/z 355.00 11.02%
147
5000 267
355 429
207
0 ‘ I 1111 i rq 111 t |'i T i" " i i •''' i ■ •' ■ i • ■ “ i • • • ■ i
m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 22.00 22.20 22.40 22.60 22.80
2152.D 5080302.M Mon Mar 18 08:30:31 2002 Page 10
NYC-WTC_000010502
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