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GCMS analysis report for sample AE02334, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010488–000010512

Folder label: “GCMS X 1/31/02 A 3/4/02

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Scanned page image, NYC-WTC_000010502
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\030402\2152.D Vial: 6 Acq On : 4 Mar 2002 2:21 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 8 Iron, monocarbonyl-(1,3-but... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.41 2.64 ug/L 1404560 Phenanthrene-dl0 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 83 2 BISTRIMETHYLSILYL N-ACETYL EICOS. . . 511 C28H57NO3Si2 000000-00-0 45 3 1,1,1,5,7,7, 7-Heptamethyl-3,3-bi... 444 C13H40O5S16 038147-00-1 42 4 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 42 Abundance Scan 2132 (22.414 min): 2152.D (-) m/z 73.10 100.00% 73

5000 147 221 281 355 429 22.00 22.20 22.40 22.60 22.80 - m/z 147.10 30.42% 0-— p*r mmmmpmmmmmmmg m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butediene-1.4-dlcarix>nic ... 73

147 221 5000 355 22.00 22.20 22.40 22.60 22.80 281 429 m/z 221.10 22.03% 26 111 503

/z—> 0 .h/u834/, — 43174/4.7 ftmme 577 652 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dlf l 73 T‘ i ■»> * i > > • > i»■ • ■ i 22.00 22.20 22.40 22.60 22.80 5000 m/z 429.10 11.11% 174 129 337 221 281 , 429 0- 44 **13901., i' • ■ ■ i ■ " • i ■" ■ i m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... 73 22.00 22.20 22.40 22.60 22.80 m/z 355.00 11.02% 147 5000 267 355 429 207

0 ‘ I 1111 i rq 111 t |'i T i" " i i •''' i ■ •' ■ i • ■ “ i • • • ■ i m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 22.00 22.20 22.40 22.60 22.80

2152.D 5080302.M Mon Mar 18 08:30:31 2002 Page 10

NYC-WTC_000010502

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NYC-WTC_000010502Source: NYC Law Department, mirrored locally

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