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GCMS analysis report, sample AE02338, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010585–000010609

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2338.D Vial: 10 Acq On 4 Mar 2002 5:38 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 11 Iron, monocafbonyl-(1,3-but... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.01 1.29 ug/L 626957 Phenanthrene- dl 0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 iron, monocarbonyl-(1,3-butadien— 438 C21H22FeN2O5 109007-87-6 45 2 Trisiloxane, 1,1,1,5,5,5-hexamet. .. 384 C12H36O4S15 003555-47-3 37 3 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207S17 071579-69-6 37 4 1H-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 32 Abundance Scan 2528 (26.005 min): 2338.D (-) m/z 73.10 100.00% 73

5000 147 221 355 281

m/z—> 0- — TP*r + —P 429 Ff*mmmpmmmp 50 100 150 200 250 300 350 400 450 500 550 600 650 25.60 25.80 26.00 26.20 26.40 m/z 147.10 40.45%

Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73

147 221 5000 355 281 25.60 25.80 26.00 26.20 26.40 429 m/z 355.10 33.36% 503 26 111 miz-> 0- —44441834 — —3174 577 652 | 1 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147

281 25.60 25.80 26.00 26.20 26.40 5000 m/z 221.10 31.91%

369 207

m/z-> 0- 2741 rr** + 24% 108. TTTUTr " I " “ I ‘ i' ■ ■ • i “ ‘' i ■' ■11 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #379639:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73 TTTTTT T T 25.60 25.80 26.00 26.20 26.40 m/z 281.10 23.51%

5000 147

221 281 ™ , 0 TT . . it 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 25.60 25.80 26.00 26.20 26.40

2338.D 5080302.M Mon Mar 18 08:32:21 2002 Page 13

NYC-WTC_000010602

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NYC-WTC_000010602Source: NYC Law Department, mirrored locally

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