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GCMS quantitative results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report listing concentrations of volatile organic compounds in sample AE03799 analyzed on March 22, 2002.

NYC-WTC_000037870–000037883

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

$ Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031902\3799.D Vial: 9 Acq On : 19 Mar 2002 6:13 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 6 Iron, monocarbonyl-(1,3-but... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.39 0.55 ug/L 339121 Phenanthrene-dl0 22.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 47 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 42 3 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 40 4 1,1,1,5,7,7, 7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 35 Abundance Scan 2129 (22.387 mln): 3799.D (-) m/ z 73.10 100.00% 73

5000 147 221 22.00 22.20 22.40 22.60 22.80 281 355 429 m/z 147.10 27". 68% 0-T T — 1 , m— A I-?! — 4 — — p — - — mlz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic... 73

147 221 ................ ............................ 5000 355 22 00 22.20 22.40 22.60 22.80 281 429 m/z 221.10 23".68% 503 26 111 0 ulau,1831.,4131711 — _ 577 652 m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE 73

22.00 22.20 22.40 22.60 22.80 m/z 355.10 10.35% 5000 174 129 337 2211 281 , 429 0-T —4 4 Hr -4 rH 390 I I ■" ■ i'1'111 ■1 ■ I mlz-? 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #380705: F2A 13.14-H2 ME ESTER 3TMS TTI—01f 73 11 •1 ‘ I ‘ ‘ 22.00 22.20 22.40 22.60 22.80 m/z 429.10 10 .00%

5000 173 224

129 20 320 429 m/z-> 14 0 TMT 0 hhaualllala 4 —P44 50 100 150 200 250 300 350 400 450 500 550 600 650 500 TTfutr • i ‘ “ i “ 1') “ PPP — ■ — .’T 22.00 22.20 22.40 22.60 22.80

3799.D 5080302.M Thu Mar 21 11:39:35 2002 Page 8

NYC-WTC_000037882

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NYC-WTC_000037882Source: NYC Law Department, mirrored locally

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