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GCMS analysis results for sample AE03282, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE03282 conducted on March 29, 2002.

NYC-WTC_000011437–000011450

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011449
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

.♦Data File : C:\MSDCHEM\1\DATA\031902\3282.D Vial: 36 Acq On : 21 Mar 2002 11:07 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 6 Iron, monocarbonyl-(1,3-but... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.40 0.58 ug/L 698750 Phenanthrene-dl 0 22.51

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 74 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 59 3 3-Isopropoxy-1,1,1,7,7,7-hexamet. . . 576 C18H52O7Si7 071579-69-6 43 4 2H-1,4-Benzodiazepin-2-one, 7-ch... 430 C21H27C1N202Si2 055319-93-2 43 Abundance Scan 2130 (22.396 min): 3282.D (-) m/z 73.10 100.00% 73

5000 147 i ■ ■ . i1 • . ... 221 29. 355 429 m ALL 22.00 22.20 22.40 22.60 22.80 T**r m/z 147.10 31.98% 0- Th m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73

147 221 5000 355 281 429 22.00 22.20 22.40 22.60 22.80 m/z 221.10 24.79% 503 26 111 m/z—> 0 434 T MU *IAmmo 577 652 [

50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DI(- 73 T T 4 T I’r 22.00 22.20 22.40 22.60 22.80 5000 m/z 429.10 14.44% 174 129 337 221 281 . 429

m/z-> 0- -14444 4 50 100 150 200 250 300 350 400 450 500 550 600 650 ...........................

Abundance #379639:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... p ‘ ' l ' >■ /) 73 i ■ • ■ ■ i ■ ■ 22.00 22.20 22.40 22.60 22.80 m/z 355.10 14.08%

5000 147

221 281 2 . J | 327 415 519 561 0 T » « I « » i :» » • jr« : j t । r • j » n ? । » » » »| \ Vi । i r j tPrt i i ] f i i r | 11 i i j i >' m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 22.00 22.20 22.40 22.60 22.80

3282.D 5080302.M Mon Mar 25 09:05:17 2002 Page 8

NYC-WTC_000011449

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NYC-WTC_000011449Source: NYC Law Department, mirrored locally

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