Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
NYC-WTC_000037948–000037963Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\031902\3804.D Vial: 14 Acq On : 19 Mar 2002 10:18 pm Operator: McLean Sample : RE-INJ 2/20 Inst ; Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Iron, monocarbonyl-(1,3-but... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.39 0.68 ug/L 314000 Phenanthrene-dlO 22.50
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 43 2 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 42 3 1,1,1,5,7,7,7-Heptamethyl-3 ,3-bi. . . 444 C13H4005Si6 038147-00-1 42 4 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 38 Abundance Scan 2129 (22.387 min): 3804.D (-) m/z 73.10 100.00% 73
5000 147 221 281 355 429 22.00 22.20 22.40 22.60 22.80 Tpurer — — . Tfur m/z 147.10 29.31% 0—T — m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73
221 5000 147 355 ... —A 22.00 22.20 22.40 22.60 22.80 • i1 1 281 429 m/z 221.10 24.14% 26 141 I 503
0- .577 Tmmfo652 miz-> i0 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundancei #380705: F2A 13,14-H2 ME ESTER 3TMS 73
22.00 22.20 22.40 22.60 22.80 50001 m/z 429.10 13.28% 173 224 320 129 260 429
m/z—> 0 aul(. 14.50+4100l150 0 36 .4...... 200 250 300 350 400 450 500 550 600 650 Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... 73 I ‘ 111111 P ' ‘ i ‘ ‘ 22.00 22.20 22.40 22.60 22.80 ■ i ‘'
m/z 355.10 11.53% 147 5000 267 355 429 207
miz—> 0 I' " ' I ’’I 1 -rp-rr f‘rm-p-r TTUuutauta"r 0 50 100 150 200 250 300 350 400 450 500 550 600 650 TTTTIr TPTT 22.00 22.20 22.40 22.60 22.80
7°0A n 580302.M Thu Mar 21 11:48:10 2002 Page 8 NYC-WTC_000037960
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NYC-WTC_000037870
Laboratory report listing concentrations of volatile organic compounds in sample AE03799 analyzed on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037906
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037964
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03805 conducted on March 22, 2002.
Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037935
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03803 conducted on March 22, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012129
Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011437
Laboratory report documenting GCMS analysis of environmental sample AE03282 conducted on March 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011415
Laboratory report documenting GCMS analysis of environmental sample AE03281 conducted on March 29, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010659
Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012182
Laboratory report for GC/MS analysis of sample AE01647 conducted on March 25, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010537
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010558
Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
Filed in the same folder
NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
Filed in the same folder
NYC-WTC_000037825
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
Filed in the same folder
NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
Filed in the same folder
NYC-WTC_000037837
Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
Filed in the same folder