Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.
NYC-WTC_000037884–000037905Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\3800.D Vial: 10 Acq On : 19 Mar 2002 7:02 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 9 F2A 13,14-H2 ME ESTER 3TMS Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.39 3.90 ug/L 2015480 Phenanthrene-dl0 22.50
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 F2A 13.14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 42 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 42 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 40 4 Iron, monocarbonyl-(1,3-butadien.•. 438 C21H22FeN2O5 109007-87-6 40 Abundance Scan 2129 (22.387 min): 3800.D (-) m/z 73.10 100.00% 73
5000 147 221 281 355 429 22.00 22.20 22.40 22.60 22.80
rn/z-> O-1T 0 45 — 50 — 117 100 150 200 250 300 350 400 450 ,1911.,249.1325— 401 500 m/z 147.10 29.82%
Abundance #380705: F2A 13.14-H2 ME ESTER 3TMS 73
5000 । * * *11 • * * * T • । <.». ।> 173 224 259 22.00 22.20 22.40 22.60 22.80 m/z 221.10 21.86% 129 320 355 429 0 —tt 1491444411+42914384 11500, 14 m/z—> ।0 50 100 150 200 250 300 350 400 450 500 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE 73
22.00 22.20 22.40 22.60 22.80 m/z 429.10 12.18% 5000 174 129 337 221 281 ■ 0T , , , ulda.. 429
miz—> 0 — 349.1,309 369 - TPgT 50 100 150 200 250 300 350 400 450 500 Abundance #352530: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... — — 73 1 ■ ■ ■ ■ I ’' ■ 22.00 22.20 22.40 22.60 22.80 m/z 355.10 11.67% 147 5000 267 355 429 207
0 r1 ‘11 TPIT P m/z—> 0 50 100 150 200 250 300 350 400 450 500 22.00 22.20 22.40 22.60 22.80
3800.D 5080302.M Thu Mar 21 11:42:26 2002 Page 11 NYC-WTC_000037897
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NYC-WTC_000037906
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037948
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037848
Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010585
Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010488
Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010513
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011347
Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010537
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010659
Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012129
Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010558
Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
Filed in the same folder
NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
Filed in the same folder
NYC-WTC_000037825
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
Filed in the same folder
NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
Filed in the same folder
NYC-WTC_000037837
Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
Filed in the same folder