Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.
NYC-WTC_000037884–000037905Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\3800.D Vial: 10 Acq On : 19 Mar 2002 7:02 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 8 Phenethylamine, N-methyl-.b... Concentration Rank 3
R.T. EstConc Area Relative to I STD R.T.
20.28 4.93 ug/L 2524800 Acenaphthene -dl0 18.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3S13 010538-85-9 35 2 N-(Trifluoroacetyl) -0,0',0'1-tri... 481 C19H34F3NO4Si3 000000-00-0 35 3 N-(Trifluoracetyl)-0,0',O''-tris... 495 C20H36F3N04Si3 054135-51-2 35 4 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12Sil2 018919-94-3 35 Abundance Scan 1897 (20.282 mln): 3800.D (-) m/z 73.10 100.00% 73
5000' 147 221 281 401 355 m 20.00 20.20 20.40 20.60 45 0-- 117 191 4—+19144249+ 327 । T TT — T1 m/z 355.10 33.16% miz-> 50 100 150 200 250 300 350 400 450 Abundance #331718: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73
—i—
5000 355 20.00 20.20 20.40 20.60 44 m/z 147.10 29.08%
i „ 116,147 •193220 267294 0- 1*’ 94 TTI iIrT’T .ii TUrugtr । . |»i ।384 >।।i।।।।।।।।।> rn/z-> 50 100 150 200 250 300 350 400 450 Abundance #364172: N-(Trifluoroacetyl)-O,O'tO"-tris(trimethylsilyl)... 73 -- 355 20.00 20.20 20.40 20.60 m/z 221.10 24.31% 5000
45 . 120147 193 236265 481 0- —U—r h r । . I 'r . . i TT TTTIe r । . , — m/z-> 50 100 150 200 250 300 350 400 450 Abundance #367529: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsllyi)e... ----- 73 20.00 20.20 20.40 20.60 m/z 281.00 15.77% 355
5000
45 —110 140 184 221 251 281 324 480 — O' .............................................................. 1 111 ’ i ■ • ■ • i • • miz--> 50 100 150 200 250 300 350 400 450 20.00 20.20 20.40 20.60
3800.D 5080302.M Thu Mar 21 11:42:25 2002 Page 10 NYC-WTC_000037896
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NYC-WTC_000037906
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037948
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037848
Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010585
Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010488
Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010513
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011347
Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010537
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010659
Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012129
Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010558
Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
Filed in the same folder
NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
Filed in the same folder
NYC-WTC_000037825
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
Filed in the same folder
NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
Filed in the same folder
NYC-WTC_000037837
Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
Filed in the same folder