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GCMS blank analysis results for sample AE03265, March 2002

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Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011347–000011364

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011358
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C:\MSDCHEM\1\DATA\031902\0214LB.D Vial: 33 Acq On : 21 Mar 2002 5:58 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 5 Phenethylamine, N-methyl-.b... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 20.29 1.03 ug/L 1202490 Acenaphthene-dl0 18.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenethylamine, N-methyl-.beta. ,... 399 C18H37NO3S13 010538-85-9 43 2 n-Nonadecanoic acid, pentamethyl... 428 C24H5202Si2 000000-00-0 43 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 43 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005S14 000000-00-0 42 Abundance Scan 1898 (20.291 min): 0214LB.D (-) m/z 73.10 100.00% 73

5000 355 147 221 281 45 401 20.00 20.20 20.40 20.60 117. 1911 , 249, 327 I m/z 355.10 39.65% 0- — ■ i ■■ Pifi -m —*2*r m/z-> 50 100 150 200 250 300 350 400 450 Abundance #331718: Phenethylamine, N-methyl-.bete.,3,4-tris(trimethy... 73

5000 355 ‘ 1111111 PPP 20.00 20.20 20.40 20.60 44 m/z 147.10 29.73%

,1 116.147 193220 267294 , I 384........ 0- 11**19mmnr miz-> 50 100 150 200 250 300 350 400 450 Abundance #346318: n-Nonadecanoic acid, pentamethyldisilyl ester 43 73 355

20.00 20.20 20.40 20.60 147 m/z 221.10 25.22% 5000 413 203

miz-> 0- 44 50 100 245 295 325 150 200 250 300 350 400 450 'I 11 ' ' 1 11 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73 I’t 20.00 20.20 20.40 20.60 m/z 281.00 18.46%

5000 355

147 105 429457 — 193 237 267295 325 47 ......... 0 .tii •n/z-> 50 100 150 200 250 300 350 400 450 20.00 26'26 20.40 20.60

0214LB.D 5080302.M Mon Mar 25 08:59:21 2002 Page 7

NYC-WTC_000011358

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NYC-WTC_000011358Source: NYC Law Department, mirrored locally

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