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Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\3799.D Vial: 9
Acq On : 19 Mar 2002 6:13 pm Operator: McLean
Sample : RE-INJ 2/20 Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 5 Benzoic acid, 2,4-bis[(trim... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
20.28 0.74 ug/L 444677 Acenaphthene-diO 18.14
Hit# of 5 Tentative ID MW Mol Form CAS# Qual
1 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 37
2 TETRACOSAMETHYLCYCLODODECASILOXA... 888 C24H72O12S112 018919-94-3 35
3 n-Nonadecanoic acid, pentamethyl... 428 C24H5202Si2 000000-00-0 35
4 2-TRIMETHYLSILYLAMINO-l-TRIMETHY... 457 C20H43N03Si4 068595-65-3 35
Abundance Scan 1897 (20.282 min): 3799.D (-) m/z 73.10 100.00%
73
5000
147 355 —i--
221
281 20.00 20.20 20.40 20.60
0-
45
■. 1— 4.-, T P '191,
i i 117 191, 249 , 3271 ——
'1 r fr I —Tr
m/z 355.10 30.89%
m/z-> 50 100 150 200 250 300 350 400
Abundance #313243: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trim...
73
5000 ------------
355
20.00 20.20 20.40 20.60
45 m/z 147.10 28.51%
16. । 105 133,163 193 223 251 281 321
0 T Tr f—r * Trr T"p T I III |*I T I IT
m/z—> 50 100 150 200 250 300 350 400
Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclodo
73
355
_ —
20.00 20.20 20.40 20.60
147 221 281 m/z 221.10 23.13%
5000
415
4 , 385, 1 ,
191 325
45 119. - • 249
0- ■ • i 1 ■ TI T । TTT TT i ■ ' T ■ i
m/z-> 50 100 150 200 250 300 350 400
Abundance #346318: n-Nonadecanoic acid, pentamethyldisilyl ester
<0 73 355 T Tr "II T
20.00 20.20 20.40 20.60
m/z 281.00 15.49%
147
5000
413
203
miz—>
0 L hill
50 100 150
,i 245 295 325 . ■ - -
' I ■ 1 TI ■ 1’ 1’r 11
200 250 300 350 400
' ‘ i' ‘ 1 11 1 • PIr —It r«*
20.00 20.20 20.40 20.60
3799.D 5080302.M Thu Mar 21 11:39:33 2002 Page 7
NYC-WTC_000037881
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