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GCMS analysis results, Sample AE01647, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report for GC/MS analysis of sample AE01647 conducted on March 25, 2002.

NYC-WTC_000012182–000012193

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS

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Scanned page image, NYC-WTC_000012192
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\031902\1647.D Vial: 27 Acq On : 20 Mar 2002 12:10 pm Operator: McLean Sample : RE-INJ 3/1 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 4 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

20.28 0.44 ug/L 196637 Acenaphthene-dl0 18.13

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 45 2 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4S13 010586-16-0 38 3 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H52O7Si7 071579-69-6 37 4 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 25 Abundance Scan 1897 (20.282 min): 1647.D (-) m/z 73.10 100.00% 73

5000 147 355 221 mIIPT i ■ ■ ‘ ■ i ■'

m/z—> o0fuidluipi TP .1.". 50 100 150 200 250 300 350 400 450 500 550 401

Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclodi > ■ i1 • ■ • i • ■ ■ ■ i' ■ 20.00 20.20 20.40 20.60 m/z 355.10 27.89%

73 355

5000 147 221 281 - ‘ ■ i ■ ■ ■ ■ i ■ 20,00 20.20 20,4020.60 m/z 147.10 27.14% 415

m/z-> 0 OTT TTP UM — 1 11*1»I Hr 50 100 150 200 250 300 350 400 450 500 550 • । • • • • । ■ • ■ • । ■

Abundance #313243: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trim... 73 000 20.00 20.20 20.40 20.60 5000 m/z 221.10 20.47% 355

133 179 223 281 291 29. 0T Tir T*r —++,149/1011/18321./ 11411****8288028**g miz-> Abundance 0 50 100 150 200 250 300 350 400 450 500 550 #379639:3-isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73 M 20.00 20.20 20.40 20.60 m/z 281.00 13.64%

5000 147

221 281 29- . 41 0mPPPp l 327 hr PIII—Jmmfmmmmptn 415 .519 561 • ■ i ■ ■ ■ ■ i ■ ■ • i ■ ■' ■ i ■ ■ m/z—> 0 50 100 150 200 250 300 350 400 450 500 550 20.00 20.20 20.40 20.60

L647.D 5080302.M Thu Mar 21 06:32:10 2002 Page 6

NYC-WTC_000012192

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NYC-WTC_000012192Source: NYC Law Department, mirrored locally

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