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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010513–000010536

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54-pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 9 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

24.29 1.68 ug/L 787256 Phenanthrene-dl0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Sil2 018919-94-3 50 2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4S15 003555-47-3 43 3 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 38 4 lH-Purin-6-amine, [ (2-fluorophen... 243 C12H10FN5 074421-44-6 37 Abundance Scan 2339 (24.291 min): 2334.D (-) m/z73.10 100.00% 73

5000 147 221 281 -I l" IT 24.00 24.20 24.40 24.60 Pr +1914— 114— 32747,25,491328— 45 117 249, m/z 147.10 37.32% m/z—> 0 nid-r 50 100 150 200 250 300 350 400 450 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod ) 73 355

5000 147 221 281 1 • ‘ * t Tt T 24.00 24.20 24.40 24.60 m/z 221.10 23.94% 415

m/z-> Abundance 0- 45 • ■ 1 1 • 50 .11%, 11*,* 166 191 249 । TTTT 150 200 250 300 + 3251 TTHTnim 350 #322218: Trisiloxane, 1.1,1,5,5,5-hexamethyl-3,3-bis[(trim... 400 ,385, I 450 73 147

281 T T T 24.00 24.20 24.40 24.60 5000 m/z 281.10 22.76%

369 45 207 20 0 4 I TPmeer 117 177 1 249 310 341 1 1 ' * * 1 ' m/z-> 50 100 150 200 250 400‘450 300 350 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DII: 73 24.00 24.20 24.40 24.60 m/z 355.10 9.57%

5000 174 129 337 221 247 281

m/z—> 0 50 l 100 150 200 250 300 311.438 —45 350 400 450 429 T T 24.00 24.20 24.40 24.60 T

2334.D 5080302.M Mon Mar 18 08:31:01 2002 Page 11

NYC-WTC_000010528

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NYC-WTC_000010528Source: NYC Law Department, mirrored locally

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