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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010513–000010536

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 8 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.41 2.19 ug/L 1025010 Phenanthrene-dl0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 42 2 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 42 3 1,1,1,5,7,7, 7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 40 4 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 32 Abundance Scan 2132 (22.414 mln): 2334.D (-) m/z 73.10 100.00% 73

5000 147 221 1 • ■ • ■ । T T TrT 281 355 401 429 22.00 22.20 22.40 22.60 22.80 0hii 1 4 *P*— 249,1,325, 4.. 45 117 ... 1911 | m/z 147.10 30.28% . m/z—> 0 50 100 150 200 250 300 350 400 450 500 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dli: 70

5000 174 22*0022.20 22.40 22.60 22.80 129 337 m/z 221.10 20.94% 221

iz-> 0 0T—T 50 4 349.1399 .9.1 100 150 200 250 300 350 400 450 L 281 500 Abundance #380705: F2A 13.14-H2 ME ESTER 3TMS 73 T T T 22.00 22.20 22.40 22.60 22.80 5000 m/z 429.10 12.23% 173 224 259 129 320 429 I REE „ 14 0111 ,192+44444444444+429 I I 355384 I I 500 . Appr m/z—> 0 50 100 150 200 250 300 350 400 450 500 Abundance #352530:1,1,1,5,7.7,7-Heptamethyi-3,3-bis(Wmethylsiloxy... ............................................ 73 22'0022.20 22.40 22.6022.80 m/z 355.10 11.09% 147 5000 267 355 429 207

- 0TTTT *I’***I*’’’I* 1 ■ i • ■ ■ i ■ ■ ■ i ■ • ■ ■ i ‘ ‘ 1 I r 1 1 11 ' ' m/z—> 0 50 100 150 200 250 300 350 400 450 500 22'06 22.20 22.40 22.60 22*80

2334.D 5080302.M Mon Mar 18 08:31:00 2002 Page 10

NYC-WTC_000010527

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NYC-WTC_000010527Source: NYC Law Department, mirrored locally

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