NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14
Acq On 4 Mar 2002 8:54 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 8 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.41 2.19 ug/L 1025010 Phenanthrene-dl0 22.52
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 42
2 F2A 13,14-H2 ME ESTER 3TMS 586 C30H62O5Si3 000000-00-0 42
3 1,1,1,5,7,7, 7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 40
4 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 32
Abundance Scan 2132 (22.414 mln): 2334.D (-) m/z 73.10 100.00%
73
5000
147
221 1 • ■ • ■ । T T TrT
281 355 401 429 22.00 22.20 22.40 22.60 22.80
0hii 1 4 *P*— 249,1,325, 4..
45 117
... 1911 | m/z 147.10 30.28%
.
m/z—> 0 50 100 150 200 250 300 350 400 450 500
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dli:
70
5000
174 22*0022.20 22.40 22.60 22.80
129 337 m/z 221.10 20.94%
221
iz-> 0
0T—T
50
4 349.1399 .9.1
100 150 200 250 300 350 400 450
L 281
500
Abundance #380705: F2A 13.14-H2 ME ESTER 3TMS
73
T T T
22.00 22.20 22.40 22.60 22.80
5000 m/z 429.10 12.23%
173 224
259
129 320
429 I REE
„ 14
0111 ,192+44444444444+429 I I 355384 I I
500 .
Appr
m/z—> 0 50 100 150 200 250 300 350 400 450 500
Abundance #352530:1,1,1,5,7.7,7-Heptamethyi-3,3-bis(Wmethylsiloxy... ............................................
73 22'0022.20 22.40 22.6022.80
m/z 355.10 11.09%
147
5000 267
355 429
207
-
0TTTT *I’***I*’’’I* 1 ■ i • ■ ■ i ■ ■ ■ i ■ • ■ ■ i ‘ ‘ 1 I r 1 1 11 ' '
m/z—> 0 50 100 150 200 250 300 350 400 450 500 22'06 22.20 22.40 22.60 22*80
2334.D 5080302.M Mon Mar 18 08:31:00 2002 Page 10
NYC-WTC_000010527
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