NYC-WTC_000011437
Laboratory report documenting GCMS analysis of environmental sample AE03282 conducted on March 29, 2002.
Same agency, volume and box · similarity 0.998
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GCMS analysis results for sample AE03281, March 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of environmental sample AE03281 conducted on March 29, 2002.
NYC-WTC_000011415–000011428Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report . Data File : C:\MSDCHEM\l\DATA\031902\3281.D Vial: 35 Acq On : 21 Mar 2002 9:11 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 6 BISTRIMETHYLSILYL N-ACETYL .. Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
22.40 0.42 ug/L 604098 Phenanthrene - d 10 22.52
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 64 2 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 56 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5S16 038147-00-1 40 4 SILICATE ANION TETRAMER 888 C24H72012Si12 000000-00-0 38 Abundance Scan 2130 (22.395 min): 3281 .D (-) m/z 73.10 100.00% 73
5000 147 221 429 i • * ■ ■ i T T 281 355 22.00 22.20 22.40 22.60 22.80
m/z-> 0JTI— np*r —— lakirt ■ i ■'" i “ “ i 50 100 150 200 250 300 350 400 450 500 550 600 650 " i “ i •• m/z 147.10 32.04%
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE: 73
5000 174 _. V, . 22.00 22.20 22.40 22.60 22.80 129 337 m/z 221.10 23.79% 221
m/z-> 0- Abundance ls--hLa 281 ,
50 100 150 200 250 300 350 400 450 500 550 600 650 429
#350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic... 73 I ■ ‘■ I ' ‘ PmPP— 22.00 22.20 22.40 22.60 22.80 147 221 m/z 429.10 15.22% 5000 355 281 429 503 .26 111 577 652 _ m/z-> 0- —444441834 +31444 H 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... 73 22.00 22.20 22.40 22.60 22.80 m/z 355.10 14.85% 147 5000 267 355 429 207
0 ’ 1 > » I I » I » I Uh J J » > I1T7 ■ i ■ “ 'i “ ' • i • ■ 11****+*43[*11***[* I'1 • • i1 ■ I'1'11 ‘ ‘11111 Tl/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 22.00 22.20 22.40 22.60 22.80
3281.D 5080302.M Mon Mar 25 09:04:07 2002 Page 8
NYC-WTC_000011427
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NYC-WTC_000011427Source: NYC Law Department, mirrored locally
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