Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.
NYC-WTC_000037884–000037905Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\3800.D Vial: 10 Acq On : 19 Mar 2002 7: 02 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 12 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.
27.52 2.58 ug/L 1378090 Chrysene-dl2 30.30
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3S12 000000-00-0 58 2 1,1,1,5,7,7,7-Heptamethy1-3,3-bi. . . 444 C13H40O5S16 038147-00-1 50 3 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 49 4 SILICATE ANION TETRAMER C24H72012Sil2 OOCOOO-OO-O 47 Abundance Sea 2695 27 tin): 3800.D (-) m/z 73.05 100.00% 73
5000 147 221 —i— — — —
281 355 429 27.20 27.40 27.60 27.80
m/z—> O' TIh 11Hr — L 50 100 150 200 250 300 350 400 450 500 550 600 650 m/z 147.10 41.98%
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dli: 73
5000 ------ 174 27.20 27.40 27.60 27.80 129 337 m/z 221.10 29.68% 221 281 , 429
miz-> 0 .... w + TH1.390.1...... pii l । i t I • £« i t i ।i » »1 | » » i II I I I | i i 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... 73
147 27.20 27.40 27.60 27.80 5000 267 m/z 355.10 18.21% 355 429 207
0- ‘‘1 " i ■ “ ' i • • T’ ■ i “ Tp-r I ‘ ■ 11 I ‘ 1’’110111117. TT miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic... — - mPPP 73 27.20 27.40 27.60 27.80 m/z 281.00 16.40%
147 221 5000 355 281 429 503 26 in
m/z-* 0- .ullua13... T ,. — TT 50 100 150 200 250 300 350 400 450 500 550 600 650 577 652 T T l 27.20 27.40 27.60 27.80 I
3800.D 5080302.M Thu Mar 21 11:42:32 2002 Page 14 NYC-WTC_000037900
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000037906
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037948
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037848
Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010585
Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010488
Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010513
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011347
Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010537
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010659
Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012129
Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010558
Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
Filed in the same folder
NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
Filed in the same folder
NYC-WTC_000037825
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
Filed in the same folder
NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
Filed in the same folder
NYC-WTC_000037837
Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
Filed in the same folder