NYC 9/11 Public Portal Document
Library Search Compound Report
"Data File : C:\MSDCHEM\1\DATA\030402\2334.D Vial: 14
Acq On : 4 Mar 2002 8:54 pm Operator: McLean
Sample : 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 11 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
27.56 1.56 ug/L 734944 Chrysene-dl2 30.34
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 80
2 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12S112 018919-94-3 52
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bi ... 444 C13H40O5Si6 038147-00-1 45
4 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 43
Abundance Scan 2699 (27.557 min): 2334.D (-) m/z 73.10 100.00%
73
5000 147
221
355 —PPIPITT
281 429 27.20 27.40 27.60 27.80
1911 325 401
0
45
11 ■ ' 100
117
Pr ' 11" +2494,1,412474/4 > ,79 m/z 147.10 42.84%
m/z—> 50 150 200 250 300 450
350 400
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE
73
5000
174 27.20 27.4027.60 27.80
129 337 m/z 221.10 35.65%
.103. 221 247 281
429
0 44alll 4-41884.1,-ATH
| 3111 369 406 1 452
-p -H* । । +* ■ |‘ ।
m/z-> 50 100 150 200 250 300 350 400 450
Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE S$ Cyclod >
73
355
‘I T T T IT
27.20 27.40 27.60 27.80
5000 147 221 281 m/z 355.10 24.85%
415
325
...
45 . .. , 119. ; 191
0 ’ I 1 1 ' ' I ' 1 ' 1 1 f 11%
249 । - 1385, J,
miz-> 50 100 150 200 250 300 350 400 450
Abundance #352530:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsitoxy...
73 27.20 27.40 27.60 27.80
m/z 281.00 19.97%
147
5000 267
355 429
45 207
0 TIB II T T I"
m/z—> 50 100 150 200 250 300 ' 350 400 ' 450 27.20 27.40 27.60 27.80
2334.D 5080302.M Mon Mar 18 08:31:04 2002 Page 13
NYC-WTC_000010530
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