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GCMS blank analysis results for sample AE03265, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011347–000011364

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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Scanned page image, NYC-WTC_000011363
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

‘ Data File : C:\MSDCHEM\1\DATA\031902\0214LB.D Vial: 33 Acq On : 21 Mar 2002 5:58 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 10 BISTRIMETHYLSILYL N-ACETYL .. Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

31.60 0.44 ug/L 498705 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 43 2 SILICONE POLYMER 458 C14H42O5Si6 000000-00-0 43 3 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Sil2 018919-94-3 38 4 1,1,1,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 28 Abundance Scan 3145 (31.602 min): 0214LB.D (-) m/z 73.10 100.00% 73

147 221 5000

281 355 T 11111 >< ।. AanT5i 429 31.20 31.40 31.60 31.80 32.00

m/z—> O- 50 ” / T"IPT 100 150 1 1911 71" 200 .. 250 —.374 300 11.29.1, 350 400 450 m/z 147.10 50.69%

Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE 73

5000 174 31.20 31.40 31.60 31.80 32.00 , 129 337 m/z 221.10 49.29% 103, 221247 281 429 0- 44444 188,4.1,444. T311 —te369 406 I 452 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #392084: SILICONE POLYMER 73 i a........ 31.20 3140 31.60 31.80 32.00 5000 m/z 281.10 24.96% 147

221 109 0— 43 .4150TT-T200 182 249 281___________

4 ■- • 4 -------------------------------- - f - fT m/z—> 50 100 250 300 350 400 450 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclode) 73 355 t * • ■ • j • 31.20 31.40 31.60 31.80 32.00 m/z 355.10 24.22%

5000 147 221 281

m/z-> 45 0- • i ' ' ’ ' i • 50 100 119, ■ 150 TIT 191

200 2491 rf"T 250 3251 , 385, J, 300 + 350 400 415

450 31.20 31.40 31.60 31.80 32.00

0214LB.D 5080302.M Mon Mar 25 08:59:30 2002 Page 12

NYC-WTC_000011363

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NYC-WTC_000011363Source: NYC Law Department, mirrored locally

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