GCMS analysis results for sample AE03801, March 22, 2002

NYC 9/11 Public Portal Document

b Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3801.D Vial: 11 Acq On : 19 Mar 2002 7:51 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 10 BISTRIMETHYLSILYL N-ACETYL ... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

27.53 0.70 ug/L 349735 Chrysene-dl2 30.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 80 2 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 38 3 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 35 4 Trisiloxane, octamethyl- (CAS) $— 236 C8H2402S13 000107-51-7 27 Abundance Scan 2696 (27.529 min): 3801 .D (-) m/z 73.05 100.00% 73

5000 147 221 281 355 ------ 429 27.20 27.40 27.60 27.80 0 TT^ATHr TIN m/z 147.10 43.05% ' ‘ l “ ' I ' ‘ ‘ I ' " I ‘ ‘ " I “ ‘ ‘ l ' ’ m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE 73

— 5000 174 27*20 27.40 27.60 27.80 ' 129 337 m/z 221.10 40.27% 221 281 , 429 — 1,390 | . 0- THr TTTT ’ i f i n r 111 ■ ij i n 11 > n 111 r m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic... 73 —i-------

27.20 27.40 27.60 27.80 147 221 5000 m/z 355.10 27.31% 355 281 429 26 111 503

—4504183. _____ 411 TTfnt 577 652 0- ’nfo m/z-> 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #392084: SILICONE POLYMER 73 27.20 27.40 27.60 27.80 * II m/z 281.00 23.99%

5000 147

221 109 j I 182{ 0- —** 281 - |I«i<}«t<«।«ii<। 1 m/z—> 50 100 150 200 250 300 350 400 450,500 550 600 650 27.20 27.40 27.60 27.80

2 OA1 E non no W oes MA= Deere

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