GCMS analysis report for sample AE02335, March 2002

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Data File C:\MSDCHEM\l\DATA\030402\2335.D Vial: 7 * Acq On 4 Mar 2002 3:11 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 11 BISTRIMETHYLSILYL N-ACETYL .. Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

31.63 0.61 ug/L 311695 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW Mol Form CAS# Qual

1 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 72 2 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 52 3 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 46 4 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 43 Abundance Scan 3148 (31.629 min): 2335.D (-) m/z 73.10 100.00% 73

5000 147 221 281 355 —ATTuf 429 31.40 31.60 31.80 32.00

iz-> 0 ..J. . ll. J | ’I’t ’I’T i' l. • f • i • ■ • ■ i ■ ■ ■. i ■ ■ । ■ i • ■. ■ i ■ ■ 50 100 150 200 250 300 350 400 450 500 550 600 650 m/z 147.10 47.21%

Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4.11-DIH 73

... ■/Yr, ■, ■. । . 5000 174 31.40 31.60 31.80 32.00 129 337 m/z 221.10 39.80% 221 281

m/z-> 0 ul - rrHrr , W9 429

50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbony-(1,3-butadiene-1,4-dicarbonic ... 73

221 a... 31.40 31.60 31.80 32.00 147 m/z 355.00 25.83% 5000 355 281 429 26 111 503

— wTHmr 0 -44441834. . 1 577 652 m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod > 73 355 T T k T 31.40 31.60 31.80 32.00 m/z 281.10 25.32%

5000 147 221 281

415

m/z—> 0 TTrrtr MTHm Th’r—H —+ ■ ‘ I ■ ‘■ I ‘“ I "' ‘ I' ‘ 50 100 150 200 250 300 350 400 450 500 550 600 650 -A— T 31.40 31.60 31.80 32.00

2335.D 5080302.M Mon Mar 18 08:31:31 2002 Page 13

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