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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010537–000010557

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\030402\2335.D Vial: 7 ' ‘Acq On : 4 Mar 2002 3:11 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 12 SILICONE POLYMER Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

32.83 0.70 ug/L 230837 Perylene-dl2 34.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I SILICONE POLYMER 458 C14H42O5Si6 000000-00-0 50 2 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 43 3 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 38 4 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 38 Abundance Scan 3280 (32.826 min): 2335.D (-) m/ z 73.10 100.00% 73

5000 147 221 281

+ 355 -Am*4.Mf 1 429 32.60 32.80 33.00 33.20 111 । * 1. * । 1. 11।।।।j m/z 147.10 50.23% 0- TT pH miz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #392084: SILICONE POLYMER 73

5000 147 T M 32.60 32.80 33.00 33.20 221 m/z 221.10 42.82% 281 0V—H 44= m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #177443: 1H-Purin-6-amine, [(2-fluorophenyl)methyl]- (CAS)

5000 28 73

147 221 .. Y.,... 32.60 32.80 33.00 33.20 m/z 281.00 27.54% 355 281 429 503

m/z-> 0- 0 44 * rm , 50 100 150 200 250 300 350 400 450 500 550 600 650 700 563607 653 703

Abundance #350342: Iron, monocarbonyl-(1,3-butadlene-1,4-dicarbonic ... 73 —AAAAAAA 32.60 32.80 33.00 33.20 m/ z 355.10 19.94%

147 221 5000 355 281 429 26 503 ylhs 1 u 1 577 652 m/z—> 0- ** m Anfpmmp 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 32.60 32.80 33.00 33.20 '

2335.D 5080302.M Mon Mar 18 08:31:32 2002 Page 14

NYC-WTC_000010555

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NYC-WTC_000010555Source: NYC Law Department, mirrored locally

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