GCMS analysis report for sample AE02335, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

•'Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 16 SILICONE POLYMER Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

34.99 0.66 ug/L 205078 Perylene-dl2 34.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 59 2 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 50 3 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 50 4 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H30O2S14 004342-25-0 37 Abundance Scan 3518 (34.985 min): 2334.D (-) m/z 73.10 100.00% 73

147 221 5000 281 355 ‘IT 111| 11111111111 । T 429 34.60 34.80 35.00 35.20 35.40 0-naalladanyul 1 T __ L- ... m/z 147.10 59.33% •' I ’ ‘ m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #392084: SILICONE POLYMER 73

5000i 147 . MA A. 34.60 34.80 35.00 35.20 35.40 221 m/z 221.10 50.98% 109 281

miz-> 0- ,1180987,197/ -H+ i • • “ i “ ■ • i' “ ■ i “ “ i • ‘ ■411' • • i 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73 ... y... 34.60 34.80 35.00 35.20 35.40 147 221 m/z 281.00 28.83% 5000 355 281 429 503 26 111 0 —444418344 314THmmm _ 577 652 m/z--> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod > 73 355 NMndema/.VrwA 34.60 34.80 35.00 35.20 35.40 m/z 207.00 22.03%

5000

0- 147

TIH 1 — — Hrr 221 281

415 11—muuuut—B—t‘r AoT T T T T m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 34.60 34.80 35.00 35.20 35.40

2334.D 5080302.M Mon Mar 18 08:31:09 2002 Page 18

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