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GCMS analysis results for sample AE03801, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.

NYC-WTC_000037906–000037926

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037924
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031902\3801.D Vial: 11 Acq On : 19 Mar 2002 7:51 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 SILICONE POLYMER Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

31.59 0.42 ug/L 212990 Chrysene-dl2 30.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 SILICONE POLYMER 458 C14H42O5Si6 000000-00-0 43 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 38 3 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 38 4 l,l,l,5,7,7,7-Heptamethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 38 Abundance Scan 3144 (31.593 min): 3801 .D (-) m/z 73.10 100.00% 73

147 221 5000 — .— 281 355 429 31.20 31.40 31.60 31.80 32.00 hl mmmmm m/z 147.10 54.33% m/z-> 0- mpH ‘II ‘ I’ ‘I‘ 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #392084: SILICONE POLYMER 73

5000 147 I" I ‘ 1 ' • 1 1 T 31.20 31.40 31.60 31.80 32.00 221 m/z 221.10 50.00% 109 281 m/z-> 0 —H +44 1821 I H44 T ‘[ 50 100 150 200 250 300 350 400 450 500 550 600 650 T T

Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DI 73 T 31.20 31.40 31.60 31.80 32.00 m/z 355.10 23.21% 5000 174 129 337 221 . । 281 . 429 0- — 44 wul A — 4 rr1390.44— .. ।.... ।.... ।.... ।. miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73 T 31.20 31.40 31.60 31.80 32.00 TIT

m/z 281.00 21.15%

147 221 5000 355 281 429

26 ill 503

0 .4,13. —— 577 652 .......1 p • • • I»• • 11 •' T miz—> 50 100 150 200 250 300 350 400 450 500 550 600 650 31.20 31.40 31.60 31.80 32.00

3801.D 5080302.M Thu Mar 21 11:44:00 2002 Page 14 NYC-WTC_000037924

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NYC-WTC_000037924Source: NYC Law Department, mirrored locally

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