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GCMS analysis results for sample AE03801, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.

NYC-WTC_000037906–000037926

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037925
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3801.D Vial: 11 Acq On : 19 Mar 2002 7:51 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

33.91 0.41 ug/L 119279 Perylene-d12 34.18

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12Sil2 018919-94-3 47 2 Mercaptoacetic acid, bis(trimeth... 236 C8H2002SSi2 006398-62-5 47 3 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 47 4 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 43 Abundance Scan 3399 (33.906 mln): 3801 .D (-) m/z 73.10 100.00% 73

147 221 5000

281 355 A AopoHA—ALMPA, 429 33.60 33.80 34.00 34.20 0 TITTTIITITII’T’T I | | I’ III ... ........ ,... .... EETEITTTIITEIITTEOETEITTTTIETET’’’’. I m/z 147.10 61.25% m/z—> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $3 Cyclodo 73 355

5000 147 221 281 TTTTrrr ' 1 1 1 1 ‘ TI 33.60 33.80 34.00 34.20 m/z 221.10 60.10% 415 oV----- - —Hr . (. .111. n 11. > i p > i. 111.11 miz—? 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #166736: Mercaptoacetic add, bis(trimethylsilyl)- 73 147 ... LL.. -rr-p-r 33.60 33.80 34.00 34.20 ' 5000 m/z 355.0026.80%

221

m/z—> 0 0 +29.totr Hrmmmmmmmm 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #177443: 1H-Purin-6-amine, [(2-fluoropheny!)methyl]- (CAS) 73 1 • i1 *1111 i1 ■ • ■ i •1 ■ * I 33.60 33.80 34.00 34.20 m/z 281.10 24.71%

28, 147 221 5000 355 281 429 503

miz—> o 0 Alll T ... 563607653 703 50 100 150 200 250 300 350 400 450 500 550 600 650 700 AAAuAMrn 33.60 33.80 34.00 34.20

R01 .D 5080302 .M Thu Mar 21 11:44:01 2002 Page 15 NYC-WTC_000037925

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NYC-WTC_000037925Source: NYC Law Department, mirrored locally

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