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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

, Data File C:\MSDCHEM\1\DATA\030402\2339.D Vial: 11 Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 11 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

31.62 0.68 ug/L 327919 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H720: 2Si2 018919-94-3 53 2 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10F 5 / 074421-44-6 53 3 SILICATE ANION TETRAMER 888 C24H72O: 2Si12 000000-00-0 45 4 SILICONE POLYMER 458 C14H42O5Si6 000000-00-0 38 Abundance Scan 3147 (31.620 min): 2339.D (-) m/z 73.10 100.00% 73

5000 147 221

281 355 ■T..i/ii.^f.-,^.-in- | 429 31.40 31.60 31.80 32.00 0- i ■' ‘111 ■ Tr TT ’*1’3 ’T’ f !.. [.. t. t.,., ।> i > । > > 11111 > > । n 11 j i > n m/z 147.10 49.86% m/z—> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cycled ) 73 355

5000 147 221 281 32.00 31.40 31.60 31.8043.14% m/z 221.10 415 0 TBph nprt tt — —Hr ’"’B——080000103310777T0T miz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #177443: 1H-Purin-6-amine, [(2-fluorophenyl)methyl]- (CAS) 73 .... .. .......

28 147 31.40 31.60 31.80 32.00 221 m/z 281.00 22.00% 5000 355 281 429 503

m/z-> 0 0 „A Mhe d . + al 4 TIT"gggn 563607 653 703 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance 73 #391009: SILICATE ANION TETRAMER /y....... 1 ■ ■ ■ ■ । ■ ■ ■ • । • A— 31.40 31.60 31.80 32.00 m/z 355.00 17.54%

5000 147

221

n/Z—> oV 0 28 4 ... .. . 21401 50 100 150 200 250 300 350 400 450 500 550 600 650 700 . N. 31.40 31.60 31.80 32.00

2339.D 5080302.M Mon Mar 18 08:32:50 2002 Page 13

NYC-WTC_000010627

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NYC-WTC_000010627Source: NYC Law Department, mirrored locally

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