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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\030402\2339.D Vial: 11 Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 10 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

28.99 0.85 ug/L 411731 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 70 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57N03Si2 000000-00-0 50 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bi. . . 444 C13H4005S16 038147-00-1 45 4 Iron, monocarbonyl-<1,3-butadien... 438 C21H22FeN205 109007-87-6 43 Abundance Scan 2857 (28.990 min): 2339.D (-) m/z 73.10 100.00%l 73

5000 147 221 281 - — j . । / ______ । ,TTTj-r-n-i । i r 355 28.60 28.80 29.00 29.20 29.40 45 117 , t 327, | 401 429 m/z 147.10 42.83 m/z—> 0 I ‘ 50 100 ""s 150 ■ 1914 200 hij 250 A 300 350 400 450 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod ) 73 355

5000 147 221 281 / 28.60 28.80 29.00 29.20 29.40 m/z221.10 36.05? 415 191 325 45 ''I ' 1 t 119, - 1 " ''l < ■ a1 Jr i 1,385,1, "IB 249 i m/z—> 50 100 150 200 250 300 350 400 450 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE: 73 ...... ..... .......

28.60 28.80 29.00 29.20 29.40 5000 m/z 281.00 22.32? 174 129 337 103, 221 247 281 429 0- , 4,46,444 44,188,.,,11.4.311 , 369 406 L 452 Th i i । ! i l‘ । m/z-> Abundance 50 100 150 200 250 300 350 400 #352530:1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiloxy... 73 450 T • I • ' y...... I • ' ’ ’ I ' ’ ' n • ’ 28.60 28.80 29.00 29.20 29.40 m/z 355.00 16.14? 147 5000 267 355 429 45 207

0 ‘i • ■ ■ • I ■ ■ • ■ i • ■ l‘ ( • i ‘ ‘ • i ' ’ I' ■ ■ ■ i ■ ’ ■ i ■ i1 ■ ‘ ■ i • • i111 ■ l ■ • /z—> 50 100 150 200 250 300 350 400 450 28.60 28.80 29.00 29.20 29.40

2339.D 5080302.M Mon Mar 18 08:32:48 2002 Page 12

NYC-WTC_000010626

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NYC-WTC_000010626Source: NYC Law Department, mirrored locally

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