NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\030402\2339.D Vial: 11
Acq On 4 Mar 2002 6:27 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 10 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
28.99 0.85 ug/L 411731 Chrysene-dl2 30.34
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 70
2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57N03Si2 000000-00-0 50
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bi. . . 444 C13H4005S16 038147-00-1 45
4 Iron, monocarbonyl-<1,3-butadien... 438 C21H22FeN205 109007-87-6 43
Abundance Scan 2857 (28.990 min): 2339.D (-) m/z 73.10 100.00%l
73
5000 147
221
281 -
— j
. ।
/ ______
। ,TTTj-r-n-i । i r
355
28.60 28.80 29.00 29.20 29.40
45 117 , t 327, | 401 429 m/z 147.10 42.83
m/z—>
0 I ‘
50 100
""s
150
■ 1914
200
hij
250
A 300 350 400 450
Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod )
73 355
5000 147 221 281 /
28.60 28.80 29.00 29.20 29.40
m/z221.10 36.05?
415
191 325
45
''I ' 1
t 119, - 1 " ''l < ■ a1 Jr i 1,385,1, "IB
249 i
m/z—> 50 100 150 200 250 300 350 400 450
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE:
73 ...... ..... .......
28.60 28.80 29.00 29.20 29.40
5000 m/z 281.00 22.32?
174
129 337
103, 221 247 281
429
0- , 4,46,444 44,188,.,,11.4.311 , 369 406 L 452
Th i i । ! i l‘ ।
m/z->
Abundance
50 100 150 200 250 300 350 400
#352530:1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethylsiloxy...
73
450
T • I • '
y......
I • ' ’ ’ I ' ’ ' n • ’
28.60 28.80 29.00 29.20 29.40
m/z 355.00 16.14?
147
5000 267
355 429
45 207
0 ‘i • ■ ■ • I ■ ■ • ■ i • ■ l‘ ( • i ‘ ‘ • i ' ’ I' ■ ■ ■ i ■ ’ ■ i ■ i1 ■ ‘ ■ i • • i111 ■ l ■ •
/z—> 50 100 150 200 250 300 350 400 450 28.60 28.80 29.00 29.20 29.40
2339.D 5080302.M Mon Mar 18 08:32:48 2002 Page 12
NYC-WTC_000010626
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