NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\030402\2152.D Vial: 6
Acq On 4 Mar 2002 2:21 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 13 1,1,1,5,7,7,7-Heptamethyl-3... Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
31.63 1.36 ug/L 684141 Chrysene-dl2 30.34
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bi. . . 444 C13H4005Si6 038147-00-1 37
2 TETRACOSAMETHYLCYCLCTOODECASILOXA... 888 C24H72012Sil2 018919-94-3 35
3 BISTRIMETHYLSILYL NF ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 35
4 Iron, monocarbonyl-/(l,3-butadien... 438 C21H22FeN205 109007-87-6 35
Abundance Scan 3148 (31.629 min): 2152.D (-) m/z 73.10 100.00%
73
147
5000 221
281 355
r > mi . f । tirome [ .->
429 31.40 31.60 31.80 32.00
m/z->
0- 1 I ’ 1
50 100
—1174+
150
-PejA-Pri l
200
.
191
,4/1,4,3274
250 300 350 400 450
, 401 m/z 147.10 57.14%
Abundance #352530: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy...
73
147
5000 267 T Y T T
355 429 31.40 31.60 31.80 32.00
45 207 m/z 221.10 43.72%
0 •#+***I‘*‘*I*’ 1‘*‘‘1‘***}****I*‘*‘1**‘*I*
m/z—> 50 100 150 200 250 300 350 400 450
Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cycled )
73
355
■ ■ ■ • । > • i ■ • Yi r... j. ।.
31.40 31.60 31.80 32.00
5000 147 221 281 m/z 355.10 26.06%
415
191 325
45
0 ■'i * ■ • ■ i 119 — —249 IB । it .385] |
* ’ i • ' i ■ • • ■ i •
m/z-> 50 100 150 200 250 300 350 400 450
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dlii .............. \...............
73 31.40 31.60 31.80 32.00
m/z 281.00 25.46%
5000
174
. 129 337
103, 221 247 281
0 4 hal 4 4 | .188—+ "TTTr
1 ...3111
III 4 THTt—T
1369 406429452
Mfipui
m/z—> 50100 150 * 200 250 300 350 400 450
• ■ i ‘1 ■ ' i
31.40 31.60 31.80 32.00
2152.D 5080302.M Mon Mar 18 08:30:36 2002 Page 15
NYC-WTC_000010507
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