GCMS analysis report for sample AE02334, March 2002

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. Data File : C:\MSDCHEM\1\DATA\030402\2152.D Vials 6 Acq On : 4 Mar 2002 2:21 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 14 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

32.82 1.57 ug/L 521781 Perylene-dl2 34.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12Sil2 018919-94-3 49 2 Iron, monocarbony]-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 49 3 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 43 4 Trisiloxane, 1,1/1,5,5,5 -hexamet... 384 C12H3604Si5 003555-47-3 35 Abundance Scan 3279 (32.817 min): 2152.D (-) m/ z 73.05 100.00% 73

147 5000 221

281 355 429 32.40 32.60 32.80 33.00 33.20 0 TTTTTT p—*r T rrja 1 , Aik) ■ f L । i ■ ■ i | i i ■ rrrrrr : r. rj > !■ m/z 147.10 57.46% m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod ) 73 355

______ ... 5000 147 221 281 32.40 32.66 32.80 33.00 33.20 m/z221.10 49.42% 415

n/z-> 0- TThrTHr * —H ++ TH ......................... TI 50 100 150 200 250 300350400450500550600650 ■ ■ i “ ‘' i' “ 11' ■'' I'1

Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73 111 • ■ 32.40 32.60 32.80 33.00 33.20 147 221 5000 m/z 281.00 22.72% 355 281 429 26 111 503

miz-> 0- .4 44a+183. — HU TTf [ 577 652 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #392084: SILICONE POLYMER 73 InAAmaIMMAM 32.40 32.60 32.80 33.00 33.20 m/z 355.00 20.93%

5000 147

221 109 281 miz—> 0 —** 4114.197/ [d fr . 32.40 32.60 32.80 33.66 33*20 50 100 150 200 250 300 350 400 450 500 550 600 650

2152.D 5080302.M Mon Mar 18 08:30:38 2002 Page 16

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