GCMS analysis report for sample AE02335, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

.’Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 15 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

33.93 0.97 ug/L 299618 Perylene-dl2 34.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 49 2 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 47 3 SILICATE ANION TETRAMER 888 C24H72012Sil2 000000-00-0 38 4 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN205 109007-87-6 38 Abundance Scan 3402 (33.933 min): 2334.D (-) m/ z 73.10 100.00% 73

147 5000- 221

281 aP—*A1*PR 355 429 33.60 33.80 34.00 34.20 49 191 m/z 147.10 61.80% m/z—> 0- 50 100 150 1* 1 250 1 200 300 350 400 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod ) 73 355

5000 147 221 281 33.60 33.80 34.00 34.20 m/z 221.10 46.08% 415 325 0- • ■ i 1 ‘ . 45 . 119, . . 191.1 i-i । 11 "I r i ' 1 i ■ 249 — 1, 385, I . . • ■ i • • m/z-> 50 100 150 200 250 300 350 400 Abundance #392084: SILICONE POLYMER 73 ‘ I T T A T 33.60 33.80 34.00 34.20 m/z 281.00 24.39% 5000 147

221 109 43 0- • ’ I ‘ ' 249 *-4281 niz-> Abundance 50 73 100 150 200 250 300 350 #391009: SILICATE ANION TETRAMER 400 A nojutpkicooorar 33.60 33.80 34.00 34.20 m/z 355.00 18.52%

5000 147

221 28 281 401 m/z—> 0 A 50 100 150 200 250 PP1 300 350 400 - 33.60 33.80 34.00 34.20 ‘

2334.D 5080302.M Mon Mar 18 08:31:08 2002 Page 17

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