GCMS analysis report for sample AE02335, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. -Data 'Pile C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 14 Iron, monocarbonyl- (1,3-but... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

32.82 1.35 ug/L 416103 Perylene-dl2 34.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 87 2 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 43 3 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 32 4 OXID DTT 1TBDMS 1TMS 338 C13H30O2S2Si2 000000-00-0 27 Abundance Scan 3279 (32.817 mln): 2334.D (-) m/z 73.05 100.00% 73

147 5000 221 281 355 1 ■ rfm r, ■ TIRP 1 429 32.40 32.60 32.80 33.00 33.20 — m/z 147.10 56.23% 0- ■' I ■ ■'■■■ i ■ ■ T11f m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73

147 221 5000 355 1 TIPIm 32.40 32.60 32.80 33.00 33.20 281 429 m/z 221.10 42.96% 503 26 111 317.| 1 ...... 577 652 0 —4434 — m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #392084: SILICONE POLYMER 73

i ■ ■ ■ ■ I I T • i ■ ■ 32.40 32.60 32.80 33.00 33.20 5000 m/z 281.00 22.76% 147

221 109 281

m/z—> 0 mH +4182 '' '1 *4*i-| ।j।11i»» 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIIi MAMMAA . 73 32.40 32.60 32.80 33.00 33.20 m/z 355.00 20.95%

5000 174 129 337 221 281 , 429

•n/z-> 0 ..1444. rerer 3901 1’101011041’0210—229303031771’7 50 100 150 200 250 300 350 400 450 500 550 600 650 PP 32.40 32.60 32.80 33.00 33.20

2334.D 5080302.M Mon Mar 18 08:31:07 2002 Page 16

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