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GCMS analysis report, sample AE02338, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010585–000010609

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

. Data File C:\MSDCHEM\1\DATA\030402\2338.D Vial: 10 Acq On 4 Mar 2002 5:38 pm Operator: McLean Sample 1/31 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 15 Iron, monocarbonyl-(1,3-but... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

32.82 1.09 ug/L 344694 Perylene-d12 34.21

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 52 2 SILICONE POLYMER 458 C14H42O5Si6 000000-00-0 43 3 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3S12 000000-00-0 43 4 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 40 Abundance Scan 3279 (32.817 mln): 2338.D (-) m/z 73.10 100.00% 73

147 5000 221 281 355 104 | 429 32.40 32.60 32.80 33.00 33.20 0- "I"'...... br 11 r “ J * • m/z 147.10 61.15% m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73

147 221 5000 355 1/ 32.40 32.60 32.80 33.00 33.20 281 429 m/z 221.10 44.27% 26 114 503

niz-> 0- lahauad 1834.—— 4317444 — ii kmpme 577 652 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #392084: SILICONE POLYMER 73 ................ ........... ................

32.40 32.60 32.80 33.00 33.20 5000 m/z 281.00 28.35% 147

221 109 281 0- TH 110.197/ +4 m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIE 73 . ul Yy . , A . A 32.40 32*60 32.80 33.00 33.20 m/z 355.00 19.58%

5000 174 129 337 221 281

m/z—> 0 . Atluka —Hm*rmter brerM I 429 l.............. 50 100 150 200 250 300 350 400 450 500 550 600 650 .................. .......................... 32.40 32.60 32.80 33.00 33.20

2338.D 5080302.M Mon Mar 18 08:32:25 2002 Page 17

NYC-WTC_000010606

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NYC-WTC_000010606Source: NYC Law Department, mirrored locally

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