GCMS analysis report, sample AE02338, March 22, 2002

NYC 9/11 Public Portal Document Library Search Compound Report 6ata File C:\MSDCHEM\1\DATA\03 04 02\2 3 3 8.D Vial: 10 Acq On 4 Mar 2002 5:38 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 16 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

33.93 0.76 ug/L 240803 Perylene-dl2 34.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 70 2 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 64 3 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 59 4 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 43 Abundance Scan 3402 (33.933 mln): 2338.D (-) m/z 73.10 100.00% 73

147 5000 221

281 355 -MmA=m*r 429 33.60 33.80 34.00 34.20

m/z-> 0 TTTmI] 4 50 100 150 200 250 300 350 400 450 500 550 600 650 • • i • ■ • ■ 11 ■ ■ ■ i . i “ m/z 147.10 58.56%

Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $3 Cyclodo 73 355

5000 147 221 281 33.60 33.80 34.00 34.20 m/z 221.10 47.63% 415 0- mIH — — Hrr 1 • i1' " i • i ■' " i “ m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbony-(1,3-butadiene-1,4-dicarbonic ... 73 I • • •' I T 33.60 33.80 34.00 34.20 147 221 5000 m/z 281.00 24.07% 355 281 429 26 111 503 1 577 652 -444441934 +3174 1111M retpipjengguunpor 0- fr m/z-> Abundance 50 100 150 200 250 300 350 400 450 500 550 600 650 73 #392084: SILICONE POLYMER MAAAMAA.AMWAN, Monou 33.60 33.80 34.00 34.20 m/z 355.10 22.61%

5000 147

221

m/z—> 0 H lm#™ 109

50 100 150 200 250 300 350 400 450 500 550 600 650 i ■ ■ • ■ i ■ ■' ■ i 33.60 33.80 34.00 34.20 T

2338.D 5080302.M Mon Mar 18 08:32:26 2002 Page 18

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