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GCMS analysis report for sample AE02334, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010488–000010512

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File C: \MSDCHEM\ 1 \DATA\ 030402\2152.D Vial: 6 Acq On 4 Mar 2002 2:21 pm Operator: McLean Sample 1/31 Inst : Instrumen Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 16 Iron, monocarbonyl-(1,3-but... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

34.99 0.81 ug/L 270303 Perylene-d12 34.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual l Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN205 109007-87-6 9l 2 SILICONE POLYMER 458 C14H42O5Si6 000000-00-0 64 3 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12S112 018919-94-3 52 4 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 38 Abundance Scan 3518 (34.985 min): 2152.D (-) m/z 73.05 100.00% 73

147 5000 221

281 355 . 429 34.60 34.80 35.00 35.20 35.40 m/z 147.10 58.07% 0- Tppr T __ 1 •11'1 . । . I, . I . . । . I . । . . . , । . , . . । . . . . । I . . . ! . . m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic ... 73

5000 147 221 355 _ u, 34 60 34.80 35.00 35.20 35.40 281 429 m/z 221.10 47.76% 26 .. 503

m/z-> 0- .1— —p MU rmmpe 50 100 150 200 250 300 350 400 450 500 550 600 650 | 577 652

Abundance #392084: SILICONE POLYMER 73

T T T 34.60 34.80 35.00 35.20 35.40 5000 m/z 207.0026.52% 147

m/z—> 0 j LI 182 mH- 109 221 281 pA li'j 111 i । ■ ■ i ■ । i i ■ ■ 11 n 1111. 1111 11 ! 11 i i 111

50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod > 73 wwwW T T UT T 1‘t 355 34.60 34.80 35.00 35.20 35.40 m/z 355.00 22.04%

5000 147 221 281

415 0 TB—r T T —H 1 i A! । I i-i | A 11 p-rr 1111 > 11 n 11111 r mr i ■' ' • i • ■ • • i ‘ 1111 • m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 34.60 34.80 35.00 35.20 35.40

2152.D 5080302.M Mon Mar 18 08:30:40 2002 Page 18

NYC-WTC_000010510

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NYC-WTC_000010510Source: NYC Law Department, mirrored locally

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