NYC 9/11 Public Portal Document
Library Search Compound Report
. Data File C:\MSDCHEM\l\DATA\030402\2338.D Vial: 10
Acq On 4 Mar 2002 5:38 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 17 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T.
34.98 0.50 ug/L 158094 Perylene-dl2 34.21
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 TETRACOSAMETHYLCYCLODODECASIIiOXA. .. 888 C24H72O12Sil2 018919-94-3 50
2 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 47
3 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 45
4 SILICATE ANION TETRAMER 888 C24H72012S112 000000-00-0 38
Abundance Scan 3518 (34.985 mln): 2338.D (-) m/z 73.05 100.00%
73
147
221
5000
281 355
117 • ■ i ■ ■ ■ ■ i • ■ • • i ‘ •
429 34.60 34.80 35.00 35.20 35.40
m/z 147.10 64.32%
0 i■i ■ ■ ■■ i ■• •• TH *11n TTT
m/z—> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700
Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod >
73 355
5000 147 221 281
34.60 34.80 35.00 35.20 35.40
m/z 221.10 53.18%
415
mfa->
0 ttrgtr pt— tr —r —H ..p... ।... <(.।।.
0 50 100 150 200 250 300 350 400 450 500 550 600 650 700
Abundance #177443: 1H-Purin-6-amine, [(2-fluorophenyl)methyl]- (CAS)
73
147 34.60 34.80 35.00 35.20 35.40
28 221
5000 m/z 281.10 29.09%
355
281 429
503
0- lake HArmyn + ,, 563607 653 703
Itmu
miz—> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700
Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-DIIi
73 mtyr—M*
34.60 34.80 35.66 35.20 35.40
m/z 355.00 27.02%
5000
174
129
221 337
- 281
m/z—>
0-
0
„ull t **r mmtmmpmpm
429
50 100 150 200 250 300 350 400 450 500 550 600 650 700
T'1 1 111 ' ' *T ' ‘ I ’ ■ ' ' l ' •
34.60 34.80 35.00 35.20 35.40
2338.D 5080302.M Mon Mar 18 08:32:27 2002 Page 19
NYC-WTC_000010608
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