GCMS analysis report, sample AE02338, March 22, 2002

NYC 9/11 Public Portal Document Library Search Compound Report . Data File C:\MSDCHEM\l\DATA\030402\2338.D Vial: 10 Acq On 4 Mar 2002 5:38 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 14 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 31.62 0.98 ug/L 473087 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12SH2 018919-94-3 45 2 1-Monolinoleoylglycerol trimethy... 498 C27H5404Si2 054284-45-6 38 3 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 35 4 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 35 Abundance Scan 3147 (31,620 min): 2338.D (-) m/z 73.10 100.00% 73

5000 147 221

281 355 A--pmp 429 31.40 31.60 31.80 32.00 0 TTrh Apr H mAHhasthuape k । .... । . | i i 1 i | 11 1 1 | 1 r m/z 147.10 48.83% m/z—> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod 73 355

5000 147 221 281 __ ... . ... 31.40 31.60 31.80 32.00 m/z 221.10 43.09% 415

n/z-> 0- TTTTrr patlapinip —H —Hrr • • i • • •• i •. ■ • । 50 100 150 200 250 300 350 400 450 500 550 600 650 •i■■

Abundance #368148: 1-Monolinoleoylglycerol trimethylsilyl ether $$ 9... 73

207 31.40 31.60 31.80 32.00 5000 147 m/z 355.00 21.25%

34 281

m/z-> 0- . 493 ... . 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-clicarbonlc... 73 31.40 31.60 31.80 32*00 m/z 281.00 19.18%

147 221 5000 355 281 429 503

m/z—> 0 26 111 444/u1831.,431744l ii 50 100 150 200 250 300 350 400 450 500 550 600 650 1 577 652 A r-T-Ti-p-r ■ 1. .. 31.40 31.60 31.80 32.00

2338.D 5080302.M Mon Mar 18 08:32:24 2002 Page 16

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