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GCMS analysis report, sample AE02338, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010585–000010609

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\030402\2338.D Vial: 10 Acq On : 4 Mar 2002 5:38 pm Operator: McLean Sample : 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 13 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

28.99 1.20 ug/L 580428 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012SH2 018919-94-3 86 2 SILICATE ANION TETRAMER 888 C24H72012S112 000000-00-0 59 3 SILICONE POLYMER 458 C14H42O5Si6 000000-00-0 43 4 1H-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 40 Abundance Scan 2857 (28.989 min): 2338.D (-) m/z 73.10 100.00% 73

5000 147 221 281 . . ... .. . 355 28.66 28.80 29*66 29.20 29.40 . 1 . 429 J 1 32544, 491., | , m/z—> 0 45 . 1 ‘T ' 1 50 117 100 150 4.11914 200 ..... 250 . 300 350 400 m/z 147.10 43.24%

Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cycled, > 73 355

147 221 281 ... . 5000 28.60 28.80 29.00 29.20 29.40 m/z 221.10 38.55% 415 325 0- T 1‘11 1 . t 119, 45 191 249 । II‘ 41 1 385, । m/z-> 50 100 150 200 TTfr 250 ’r 300 350 400 Abundance #391009: SILICATE ANION TETRAMER 73

28.60 28.80 29.00 29.20 29.40 5000, 147 m/z 281.10 20.65%

221 28 281 401 o1 I । _______ , — -11 • ■ i ■ ■ ■ 1 1 1 1 1 1 1 1 n/z-> 50 100 150 200 250 300 350 400 ...... ........... Abundance #392084: SILICONE POLYMER 73 28.60 28.80 29.66 29.20 29.40 m/z 355.10 16.39%

5000, 147

221 109 ...................... ...................... 43 m/z-> 0 - 50 rkal 100 —— 150 182 4 249 200 IPTT 221 250 300 350 400 28.60 28.80 29.00 29.20 29.40

2338.D 5080302.M Mon Mar 18 08:32:23 2002 Page 15

NYC-WTC_000010604

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NYC-WTC_000010604Source: NYC Law Department, mirrored locally

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