GCMS analysis report for sample AE02334, March 2002

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Library Search Compound Report

. Data File C:\MSDCHEM\l\DATA\030402\2152.D Vial: 6 Acq On 4 Mar 2002 2:21 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C: \DATABASE\WILEY7N. L

Peak Number 11 Iron, monocarbonyl-(1,3-but... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

27.56 1.84 ug/L 924770 Chrysene-dl2 30.34

Hit# of 5 Tentative ID MW Mol Form' CAS# Qual

1 iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 53 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 50 3 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 38 4 3-Trimethylsilyloxystearic acid,... 444 C24H52O3Si2 000000-00-0 38 Abundance Scan 2699 (27.557 min): 2152.D (-) m/z 73.10 100.00% 73

5000 147 221 355 r| I I I I | 1r l p-1 . . ! 1 . . . 1 . 281 429 27.20 27.40 27.60 27.80 m/z 147.10 40.16% 0- THr TTHp]—-mm**mmmmmmmmmmmp m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #350342: Iron, monocarbonyl-(1,3-butadiene-1,4-dicarbonic... 73

221 5000 147 355 TT T T kT Ir 27.20 27.40 27.60 27.80 281 429 m/z 221.10 32.22% 503

rn/z-> 0- 26 —4443. 111 — auul 1 —tmtpmmp 577 652 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dlf • 73

■ i ‘ ■ i ‘ ■1 ■ i • • ‘ ■ i • ‘ • i ' 27.20 27.40 27.60 27.80 5000 m/z 355.10 22.45% 174 129 221 337 281 , 429 0- AHHHHk T.390. Hpin miz-> 50 100 150 200 250 300 350 400 450 500 550 600 650 Abundance #369235: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11.13, 13-te... 73 TPTTT 27.20 27.40 27.60 27.80 m/z 281.10 17.87%

5000 207

133 281 355

m/z—> 0 2,14442/1 2811 429 489 50 100 150 200 250 300 350 400 450 500 550 600 650 I TI T T 1T 27.20 27.40 27.60 27.80 TT

2152.D 5080302.M Mon Mar 18 08:30:34 2002 Page 13

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