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GCMS analysis report for sample AE02334, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010488–000010512

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File C:\MSDCHEM\l\DATA\030402\2152.D Vial: 6 Acq On 4 Mar 2002 2:21 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 TETRACOSAMETHYLCYCLODODECAS... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

26.00 1.74 ug/L 924896 Phenanthrene-d10 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Si12 018919-94-3 47 2 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207S17 071579-69-6 37 3 Benzoic acid, 2,4 -bis [K trimethyl. .. 370 C16H3004Si3 010586-16-0 32 4 SILICATE ANION TETRAM] 888 C24H72012Si12 000000-00-0 27 Abundance Scan 2527 (25.996 min): 2152.D (-) m/z 73.10 100.00% 73

5000 147 221 355 281 25.60 25.80 26.00 26.20 26.40

m/z—> OmTTe‘Pr 0 50 100 1994474 . . — 429 150 200 250 300 350 400 450 500 550 • ■ i •' ‘ ■ i m/z 147.10 35.43%

Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod) 73 355

5000 147 221 281 i1" 11 ■1 ■' i —mmp 25.60 25.80 26.00 26.20 26.40 m/z 221.10 25.01% 415

m/z-> OTT I1r 0 — —Hrr—199 —1 11" 111" " ITT 50 100 150 200 250 300 350 400 450 500 550 Abundance #379639: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73 1 ----- 25.60 25.80 26.00 26.20 26.40 m/z 355.00 21.06% 5000 147

221 281 3- .„ I — 41 n1p—*mePmm l 327 4mmmnp 5 519 561 m/z—> 0 0 50 100 150 200 250 300 350 400 450 500 550 Abundance #313243: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trim... ...../ y............. 73 25.60 25.80 26.00 26.20 26.40 m/z 281.10 18.55%

5000 355

133 20, 0--+ 179 223 281 fmepTr 321 • i > •' k i > • ■ • i ■ < •»i • • i11■1i1' A T T n/z—> 0 50 100 150 200 250 300 350 400 450 500 550 25.60 25.80 26.00 26.20 26.40

2152.D 5080302.M Mon Mar 18 08:30:33 2002 Page 12

NYC-WTC_000010504

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NYC-WTC_000010504Source: NYC Law Department, mirrored locally

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