NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\030402\2152.D Vial: 6
Acq On 4 Mar 2002 2:21 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 9 SILICONE POLYMER Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
24.29 2.00 ug/L 1064890 Phenanthrene - dl 0 22.53
Hit# of 5 Tentative., ID MW MolForm CAS# Qual
1 SILICONE POLYMER / 458 C14H42O5Si6 000000-00-0 40
2 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H36O4Si5 003555-47-3 38
3 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12S112 018919-94-3 38
4 2H-1,4-Benzodiazepin-2-one, 7-ch. . . 430 C21H27ClN2O2Si2 055319-93-2 37
Abundance Scan/2339 (24.291 min): 2152.D (-) m/z 73.10 100.00%
73
5000
147
221 281
_ 355 400 24.00 24.20 24.40 24.60
45
m/z->
0- 01 1
50
117
100
4.1784* TTI ,4,3274,4.4400912
150 200
249 ,
250 300 350
m/z147.10 37.66%
Abundance #392084: SILICONE POLYMER
73
5000 147 114114*4244-154**14**
24.00 24.20 24.40 24.60
221 m/z281.00 23.24%
109
43 182 | 249 281
0- ' ■ ** +444 T*I1+P0e9IPPnvt
miz-> 50 100 150 200 250 300 350 400
Abundance #322218: Trisiloxane, 1,1,1.5,5,5-hexamethyl-3,3-Ws((trim...
73 147
)
281 T
24.00 24.20 24.40 24.60
5000 m/z 221.10 22.55%
m/z->
0
50
+45
117
t-T-FT —Pr
100 150 200 250
207 210
—1772491
J 310 341
’ T"I * * 1 " 1 * ■ ■ 1 ■ •
300 350 400
Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclodo
369
73 • • i' T T
24.00 24.20 24.4Q 24.60
T
355
m/z 207.00 9.77%
5000 147 221 281
415
m/z->
0
45
TTI
50
—100119— 150
191
—
200
24944
250
+1350
300
325 I 385, ।
400 24.00 24.20 2440 24.60
2152.D 5080302.M Mon Mar 18 08:30:32 2002 Page 11
NYC-WTC_000010503
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