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GCMS analysis report, sample AE02338, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010585–000010609

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2338 .D Vial: 10 Acq On 4 Mar 2002 5:38 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 10 3-Isopropoxy-l,1,1,7,7,7-he... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

24.29 1.47 ug/L 716295 Phenanthrene -dl0 22.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual l 3-Isopropoxy-l,1,1,7,7,7-hexamet... 576 C18H52O7Si7 071579-69-6 47 2 SILICATE ANION TETRAMER 888 C24H72012Sil2 000000-00-0 47 3 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 35 4 Ethanedioic acid, bis(trimethyls... 234 C8H18O4Si2 018294-04-7 35 Abundance Scan 2339 (24.291 mln): 2338.D (-) m/z 73.10 100.00% 73

5000 147 221 281 T THT T 355 490 24.00 24.20 24.40 24.60

•n/z-> 117 "7 1911 251 , 01 —TH ‘ d —**11 r P ’ 11 T * * T ‘ 1 • 1 ' 50 100 150 200 250 300 350 400 450 500 "550 3251,3994 m/z 147.10 38.50%

Abundance #379639:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73

5000 ----- 147 24.00 24.20 24.40 24.60 m/z 281.10 26.13% 43 221 281 2 ... 0+ — .| | 327 415 519 561 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #391009: SILICATE ANION TETRAMER 73

24.00 2420 24.40 24.60 5000 147 m/z 221.10 24.82%

221

miz-> 01 H 28

50 100 1 281 " 11 " ■ ■ 11 401 ■ ■ 1 150 200 250 300 350 400 450 500 550 Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 24.00 24.20 24.40 24.60 m/z 207.00 10.27% 281 5000

369 27 । 207 2 0 — rrffr 117 177,-2—7 338 J........... T T T T m/z—> 50 100 150 200 250 300 350 400 450 500 550 24.00 24.20 24.40 24.60

3338.D 5080302.M Mon Mar 18 08:32:19 2002 Page 12

NYC-WTC_000010601

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NYC-WTC_000010601Source: NYC Law Department, mirrored locally

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